phenyl-methyl(2-(7-(thiophene-2-carboximidamido)-2,3,4,5-tetrahydro-1H-benzo[b]azepin-1-yl)ethyl)carbamate

Base Information

Chemical Name:phenyl-methyl(2-(7-(thiophene-2-carboximidamido)-2,3,4,5-tetrahydro-1H-benzo[b]azepin-1-yl)ethyl)carbamate
CAS No.:1063407-97-5
Molecular Formula:C₂₅H₂₈N₄O₂S
Molecular Weight:448.589
Hs Code.:

Synonyms:phenyl-methyl(2-(7-(thiophene-2-carboximidamido)-2,3,4,5-tetrahydro-1H-benzo[b]azepin-1-yl)ethyl)carbamate

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Chemical Property of phenyl-methyl(2-(7-(thiophene-2-carboximidamido)-2,3,4,5-tetrahydro-1H-benzo[b]azepin-1-yl)ethyl)carbamate

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Technology Process of phenyl-methyl(2-(7-(thiophene-2-carboximidamido)-2,3,4,5-tetrahydro-1H-benzo[b]azepin-1-yl)ethyl)carbamate

There total 5 articles about phenyl-methyl(2-(7-(thiophene-2-carboximidamido)-2,3,4,5-tetrahydro-1H-benzo[b]azepin-1-yl)ethyl)carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 53.2%

: 1063407-96-4
phenyl 2-(7-amino-2,3,4,5-tetrahydro-11H-benzo[b]azepin-1-yl)ethyl(methyl)carbamate

: methyl thiophene-2-carbimidothioate hydroiodide

: 1063407-97-5
phenyl-methyl(2-(7-(thiophene-2-carboximidamido)-2,3,4,5-tetrahydro-1H-benzo[b]azepin-1-yl)ethyl)carbamate

Guidance literature:: phenyl 2-(7-amino-2,3,4,5-tetrahydro-11H-benzo[b]azepin-1-yl)ethyl(methyl)carbamate; methyl thiophene-2-carbimidothioate hydroiodide; In ethanol; at 20 ℃;

With water; sodium carbonate; In ethanol; dichloromethane;

Reference yield:

: 1063407-93-1
N,N-dimethyl-2-(7-nitro-2,3,4,5-tetrahydro-1H-benzo[b]azepin-1-yl)ethanamine

: 1063407-97-5
phenyl-methyl(2-(7-(thiophene-2-carboximidamido)-2,3,4,5-tetrahydro-1H-benzo[b]azepin-1-yl)ethyl)carbamate

Guidance literature:: Multi-step reaction with 3 steps

1: dichloromethane / 20 °C

2: palladium on activated charcoal; hydrogen / ethanol / 20 °C

3: ethanol / 20 °C

With palladium on activated charcoal; hydrogen; In ethanol; dichloromethane;
DOI:10.1016/j.bmcl.2012.02.004

Reference yield:

: 1063407-94-2
phenyl methyl(2-(7-nitro-2,3,4,5-tetrahydro-1H-benzo[b]azepin-1-yl)ethyl)carbamate

: 1063407-97-5
phenyl-methyl(2-(7-(thiophene-2-carboximidamido)-2,3,4,5-tetrahydro-1H-benzo[b]azepin-1-yl)ethyl)carbamate

Guidance literature:: Multi-step reaction with 2 steps

1: palladium on activated charcoal; hydrogen / ethanol / 20 °C

2: ethanol / 20 °C

With palladium on activated charcoal; hydrogen; In ethanol;
DOI:10.1016/j.bmcl.2012.02.004