N-methyl-4-tert-butyl-1-cyclohexenecarboxamide

Base Information

Chemical Name:N-methyl-4-tert-butyl-1-cyclohexenecarboxamide
CAS No.:96759-30-7
Molecular Formula:C₁₂H₂₁NO
Molecular Weight:195.305
Hs Code.:

Synonyms:N-methyl-4-tert-butyl-1-cyclohexenecarboxamide

Suppliers and Price of N-methyl-4-tert-butyl-1-cyclohexenecarboxamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-methyl-4-tert-butyl-1-cyclohexenecarboxamide

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Technology Process of N-methyl-4-tert-butyl-1-cyclohexenecarboxamide

There total 1 articles about N-methyl-4-tert-butyl-1-cyclohexenecarboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 7370-14-1
4-tert-butyl-1-cyanocyclohexene

: 74-88-4
methyl iodide

: 96759-30-7
N-methyl-4-tert-butyl-1-cyclohexenecarboxamide

Guidance literature:: With silver tetrafluoroborate; In dichloromethane; for 12h; Ambient temperature;
DOI:10.1021/ja00302a024

Reference yield:

: 96759-30-7
N-methyl-4-tert-butyl-1-cyclohexenecarboxamide

: 5-tert-butyl-3,3-diphenyl-3aα,4,5α,6-tetrahydro-1(3H)-isobenzofuranone

Guidance literature:: Multi-step reaction with 2 steps

1: n-BuLi / tetrahydrofuran / 1.) 0 deg C, 15 min; 2.) -78 deg C, 1.2 h

2: 83 percent / xylene / 8 h / Heating

With n-butyllithium; In tetrahydrofuran; xylene;
DOI:10.1021/ja00302a024