Technology Process of methyl onate
There total 9 articles about methyl onate which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
N-Bromosuccinimide; molecular sieve;
In
dichloromethane;
for 2h;
Ambient temperature;
- Guidance literature:
-
Multi-step reaction with 4 steps
2: lithium naphthalenide / tetrahydrofuran
3: 1) LDA, 2) hexachloroethane / 1) THF, -70 deg C, 2) THF
4: Ag2SO4
With
hexachloroethane; silver sulfate; naphthalen-1-yl-lithium; lithium diisopropyl amide;
In
tetrahydrofuran;
DOI:10.1039/c39880000985
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 1) LDA / 1)THF, -70 deg C, 15 min, 2) -70 deg C to r.t., 1h
2: 1) lithium naphthalenide, 2) MeOH / 1) THF, -75 deg C, 5 min, 2) -75 to 0 deg C
3: 1) LDA, 2) hexachloroethane / 1) THF, -70 deg C, 20 min, 2) -70 deg C to r.t.
4: 25 percent / Ag2SO4, CaSO4, I2 / Ambient temperature
With
methanol; calcium sulfate; hexachloroethane; iodine; silver sulfate; naphthalen-1-yl-lithium; lithium diisopropyl amide;
