tert-Butyl<(tert-butylchlorphosphino)(trimethylsiloxy)methylen>phosphan

Base Information

• Chemical Name: tert-Butyl<(tert-butylchlorphosphino)(trimethylsiloxy)methylen>phosphan
• CAS No.: 80705-63-1
• Molecular Formula: C₁₂H₂₇ClOP₂Si
• Molecular Weight: 312.832

Synonyms:tert-Butyl<(tert-butylchlorphosphino)(trimethylsiloxy)methylen>phosphan

Chemical Property of tert-Butyl<(tert-butylchlorphosphino)(trimethylsiloxy)methylen>phosphan

Chemical Property:

Purity/Quality:

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Technology Process of tert-Butyl<(tert-butylchlorphosphino)(trimethylsiloxy)methylen>phosphan

There total 1 articles about tert-Butyl<(tert-butylchlorphosphino)(trimethylsiloxy)methylen>phosphan which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

tert-Butyl<(trimethylsiloxy)methylen>phosphan (80705-56-2,80705-57-3,84715-54-8) → chloro-trimethyl-silane (75-77-4) + tert-Butyl<(tert-butylchlorphosphino)(trimethylsiloxy)methylen>phosphan (80705-63-1)

Guidance literature:

With hexachloroethane; In toluene; for 0.25h; Ambient temperature; further reagent: COCl₂;

Reference yield:

tert-Butyl<(tert-butylchlorphosphino)(trimethylsiloxy)methylen>phosphan (80705-63-1) → chloro-trimethyl-silane (75-77-4) + tert-butyldichlorophosphine (25979-07-1)

Guidance literature:

With COCl₂; In toluene; for 10h; Yield given; Ambient temperature;

Reference yield:

tert-Butyl<(tert-butylchlorphosphino)(trimethylsiloxy)methylen>phosphan (80705-63-1) + 1,3-Diphenyl-2-<<4-(trifluormethyl)phenyl>(trimethylsilyl)amino>-3-(trimethylsilyl)-1,3-diphospha-1-propen (86229-56-3) → {[2-tert-Butyl-2-(tert-butylphosphanylidene-trimethylsilanyloxy-methyl)-1-phenyl-diphosphanyl]-phenylphosphanylidene-methyl}-(4-trifluoromethyl-phenyl)-trimethylsilanyl-amine + (3,5-Di-tert-butyl-2,6-diphenyl-4-trimethylsilanyloxy-2,3,5,6-tetraphospha-bicyclo[2.2.0]hex-1-yl)-(4-trifluoromethyl-phenyl)-trimethylsilanyl-amine

Guidance literature:

upstream raw materials:

tert-Butyl<(trimethylsiloxy)methylen>phosphan

Downstream raw materials:

chloro-trimethyl-silane

tert-butyldichlorophosphine

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