diethyl 3-(4-((4-(bis(4-methoxyphenyl)amino)phenyl)(4-methoxyphenyl)amino)phenoxy)propylphosphonate

Base Information

Chemical Name:diethyl 3-(4-((4-(bis(4-methoxyphenyl)amino)phenyl)(4-methoxyphenyl)amino)phenoxy)propylphosphonate
CAS No.:1206195-90-5
Molecular Formula:C₄₀H₄₅N₂O₇P
Molecular Weight:696.78
Hs Code.:

Synonyms:diethyl 3-(4-((4-(bis(4-methoxyphenyl)amino)phenyl)(4-methoxyphenyl)amino)phenoxy)propylphosphonate

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Chemical Property of diethyl 3-(4-((4-(bis(4-methoxyphenyl)amino)phenyl)(4-methoxyphenyl)amino)phenoxy)propylphosphonate

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Technology Process of diethyl 3-(4-((4-(bis(4-methoxyphenyl)amino)phenyl)(4-methoxyphenyl)amino)phenoxy)propylphosphonate

There total 13 articles about diethyl 3-(4-((4-(bis(4-methoxyphenyl)amino)phenyl)(4-methoxyphenyl)amino)phenoxy)propylphosphonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.4%

: 1206195-89-2
N₁-(4-(3-bromopropoxy)phenyl)-N₁,N₄,N₄-tris(4-methoxyphenyl)benzene-1,4-diamine

: 122-52-1
triethyl phosphite

: 1206195-90-5
diethyl 3-(4-((4-(bis(4-methoxyphenyl)amino)phenyl)(4-methoxyphenyl)amino)phenoxy)propylphosphonate

Guidance literature:: at 160 ℃; Inert atmosphere;

Reference yield: 83.4%

: 1206195-89-2
N₁-(4-(3-bromopropoxy)phenyl)-N₁,N₄,N₄-tris(4-methoxyphenyl)benzene-1,4-diamine

: 1206195-90-5
diethyl 3-(4-((4-(bis(4-methoxyphenyl)amino)phenyl)(4-methoxyphenyl)amino)phenoxy)propylphosphonate

Guidance literature:: With triethyl phosphite;

Reference yield:

: 194416-45-0
4-bromo-N,N-bis-(4-methoxyphenyl)aniline

: 1206195-90-5
diethyl 3-(4-((4-(bis(4-methoxyphenyl)amino)phenyl)(4-methoxyphenyl)amino)phenoxy)propylphosphonate

Guidance literature:: Multi-step reaction with 5 steps

1.1: tri-tert-butyl phosphine; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; sodium t-butanolate / toluene / 90 °C / Inert atmosphere

2.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 20 °C / Inert atmosphere

3.1: dmap / tetrahydrofuran / 0.17 h / Cooling with ice; Inert atmosphere

3.2: 0.17 h

3.3: 0.08 h

4.1: lithium bromide / tetrahydrofuran / 60 °C / Inert atmosphere

5.1: 160 °C / Inert atmosphere

With dmap; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; tri-tert-butyl phosphine; tetrabutyl ammonium fluoride; lithium bromide; sodium t-butanolate; In tetrahydrofuran; toluene;