3-(4-((4-(bis(4-methoxyphenyl)amino)phenyl)(4-methoxyphenyl)amino)phenoxy)propylphosphonic acid

Base Information

Chemical Name:3-(4-((4-(bis(4-methoxyphenyl)amino)phenyl)(4-methoxyphenyl)amino)phenoxy)propylphosphonic acid
CAS No.:1206195-91-6
Molecular Formula:C₃₆H₃₇N₂O₇P
Molecular Weight:640.673
Hs Code.:

Synonyms:3-(4-((4-(bis(4-methoxyphenyl)amino)phenyl)(4-methoxyphenyl)amino)phenoxy)propylphosphonic acid

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Chemical Property of 3-(4-((4-(bis(4-methoxyphenyl)amino)phenyl)(4-methoxyphenyl)amino)phenoxy)propylphosphonic acid

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Technology Process of 3-(4-((4-(bis(4-methoxyphenyl)amino)phenyl)(4-methoxyphenyl)amino)phenoxy)propylphosphonic acid

There total 13 articles about 3-(4-((4-(bis(4-methoxyphenyl)amino)phenyl)(4-methoxyphenyl)amino)phenoxy)propylphosphonic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.2%

: 1206195-90-5
diethyl 3-(4-((4-(bis(4-methoxyphenyl)amino)phenyl)(4-methoxyphenyl)amino)phenoxy)propylphosphonate

: 1206195-91-6
3-(4-((4-(bis(4-methoxyphenyl)amino)phenyl)(4-methoxyphenyl)amino)phenoxy)propylphosphonic acid

Guidance literature:: diethyl 3-(4-((4-(bis(4-methoxyphenyl)amino)phenyl)(4-methoxyphenyl)amino)phenoxy)propylphosphonate; With trimethylsilyl bromide; In dichloromethane; at 20 ℃; Inert atmosphere;

With water; In methanol;

Reference yield:

: 194416-45-0
4-bromo-N,N-bis-(4-methoxyphenyl)aniline

: 1206195-91-6
3-(4-((4-(bis(4-methoxyphenyl)amino)phenyl)(4-methoxyphenyl)amino)phenoxy)propylphosphonic acid

Guidance literature:: Multi-step reaction with 6 steps

1.1: tri-tert-butyl phosphine; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; sodium t-butanolate / toluene / 90 °C / Inert atmosphere

2.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 20 °C / Inert atmosphere

3.1: dmap / tetrahydrofuran / 0.17 h / Cooling with ice; Inert atmosphere

3.2: 0.17 h

3.3: 0.08 h

4.1: lithium bromide / tetrahydrofuran / 60 °C / Inert atmosphere

5.1: 160 °C / Inert atmosphere

6.1: trimethylsilyl bromide / dichloromethane / 20 °C / Inert atmosphere

With dmap; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; trimethylsilyl bromide; tri-tert-butyl phosphine; tetrabutyl ammonium fluoride; lithium bromide; sodium t-butanolate; In tetrahydrofuran; dichloromethane; toluene;

Reference yield:

: 20440-94-2
N,N-bis(4-methoxyphenyl)aniline

: 1206195-91-6
3-(4-((4-(bis(4-methoxyphenyl)amino)phenyl)(4-methoxyphenyl)amino)phenoxy)propylphosphonic acid

Guidance literature:: Multi-step reaction with 7 steps

1.1: N-Bromosuccinimide / N,N-dimethyl-formamide / 20 °C

2.1: tri-tert-butyl phosphine; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; sodium t-butanolate / toluene / 90 °C / Inert atmosphere

3.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 20 °C / Inert atmosphere

4.1: dmap / tetrahydrofuran / 0.17 h / Cooling with ice; Inert atmosphere

4.2: 0.17 h

4.3: 0.08 h

5.1: lithium bromide / tetrahydrofuran / 60 °C / Inert atmosphere

6.1: 160 °C / Inert atmosphere

7.1: trimethylsilyl bromide / dichloromethane / 20 °C / Inert atmosphere

With dmap; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; N-Bromosuccinimide; trimethylsilyl bromide; tri-tert-butyl phosphine; tetrabutyl ammonium fluoride; lithium bromide; sodium t-butanolate; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; toluene;