Technology Process of C9H14O3
There total 5 articles about C9H14O3 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C10H20O2Si; ethyl vinyl ether;
With
ammonium cerium(IV) nitrate; calcium carbonate;
In
ethanol;
cooling;
With
sulfuric acid;
In
1,4-dioxane;
at 20 ℃;
for 5h;
Further stages.;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: KH / tetrahydrofuran
1.2: 5.86 g / tetrahydrofuran / 18 h / 20 °C
2.1: 95 percent / aq. HCl / tetrahydrofuran / 5 h / Heating
3.1: 95 percent / triethylamine / dimethylformamide / Heating
4.1: Ce(NH4)2(NO3)6; CaCO3 / ethanol / cooling
4.2: 47 percent / aq. H2SO4 / dioxane / 5 h / 20 °C
With
hydrogenchloride; ammonium cerium(IV) nitrate; potassium hydride; triethylamine; calcium carbonate;
In
tetrahydrofuran; ethanol; N,N-dimethyl-formamide;
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: NaBH4 / methanol / 3 h / 20 °C
2.1: KH / tetrahydrofuran
2.2: 5.86 g / tetrahydrofuran / 18 h / 20 °C
3.1: 95 percent / aq. HCl / tetrahydrofuran / 5 h / Heating
4.1: 95 percent / triethylamine / dimethylformamide / Heating
5.1: Ce(NH4)2(NO3)6; CaCO3 / ethanol / cooling
5.2: 47 percent / aq. H2SO4 / dioxane / 5 h / 20 °C
With
hydrogenchloride; sodium tetrahydroborate; ammonium cerium(IV) nitrate; potassium hydride; triethylamine; calcium carbonate;
In
tetrahydrofuran; methanol; ethanol; N,N-dimethyl-formamide;