N-(2,2-dichlorovinyl)-N-(3-furan-2-yl-1-methylpropyl)-4-methylbezenesulfonamide

Base Information

• Chemical Name: N-(2,2-dichlorovinyl)-N-(3-furan-2-yl-1-methylpropyl)-4-methylbezenesulfonamide
• CAS No.: 1064781-04-9
• Molecular Formula: C₁₇H₁₉Cl₂NO₃S
• Molecular Weight: 388.315
• Mol file: 1064781-04-9.mol

Synonyms:N-(2,2-dichlorovinyl)-N-(3-furan-2-yl-1-methylpropyl)-4-methylbezenesulfonamide

Chemical Property of N-(2,2-dichlorovinyl)-N-(3-furan-2-yl-1-methylpropyl)-4-methylbezenesulfonamide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N-(2,2-dichlorovinyl)-N-(3-furan-2-yl-1-methylpropyl)-4-methylbezenesulfonamide

There total 1 articles about N-(2,2-dichlorovinyl)-N-(3-furan-2-yl-1-methylpropyl)-4-methylbezenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 21.0%

tetrachloromethane (56-23-5) + N-formyl-N-tosylamide (4917-56-0) + 4-(furan-2-yl)butan-2-ol (6963-39-9,71638-59-0) → N-(2,2-dichlorovinyl)-N-(3-furan-2-yl-1-methylpropyl)-4-methylbezenesulfonamide (1064781-04-9)

Guidance literature:

N-formyl-N-tosylamide; 4-(furan-2-yl)butan-2-ol; With di-isopropyl azodicarboxylate; triphenylphosphine; In tetrahydrofuran; at 20 ℃; for 16h;

tetrachloromethane; With triphenylphosphine; In tetrahydrofuran; at 60 ℃; for 16h;

DOI:10.1002/chem.200800210

Reference yield: 82.0%

N-(2,2-dichlorovinyl)-N-(3-furan-2-yl-1-methylpropyl)-4-methylbezenesulfonamide (1064781-04-9) → N-ethynyl-N-(3-furan-2-yl-1-methylpropyl)-4-methylbenzenesulfonamide (1064781-07-2)

Guidance literature:

With n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃; for 0.0833333h;

DOI:10.1002/chem.200800210

upstream raw materials:

tetrachloromethane

N-formyl-N-tosylamide

4-(furan-2-yl)butan-2-ol

Downstream raw materials:

N-ethynyl-N-(3-furan-2-yl-1-methylpropyl)-4-methylbenzenesulfonamide