2-(2-hydrazono-4-oxo-thiazolidin-3-yl)-6-(4-nitrophenylthio)benzthiazole

Base Information

• Chemical Name: 2-(2-hydrazono-4-oxo-thiazolidin-3-yl)-6-(4-nitrophenylthio)benzthiazole
• CAS No.: 296232-32-1
• Molecular Formula: C₁₆H₁₁N₅O₃S₃
• Molecular Weight: 417.493

Synonyms:2-(2-hydrazono-4-oxo-thiazolidin-3-yl)-6-(4-nitrophenylthio)benzthiazole

Chemical Property of 2-(2-hydrazono-4-oxo-thiazolidin-3-yl)-6-(4-nitrophenylthio)benzthiazole

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Technology Process of 2-(2-hydrazono-4-oxo-thiazolidin-3-yl)-6-(4-nitrophenylthio)benzthiazole

There total 1 articles about 2-(2-hydrazono-4-oxo-thiazolidin-3-yl)-6-(4-nitrophenylthio)benzthiazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

2-(2'-thioxo-4'-oxo-thiazolidin-3'-yl)-6-(p-nitrophenylthio)benzthiazole (134961-34-5) → 2-(2-hydrazono-4-oxo-thiazolidin-3-yl)-6-(4-nitrophenylthio)benzthiazole (296232-32-1)

Guidance literature:

With hydrazine hydrate; In 1,4-dioxane; ethanol; at 20 ℃; for 10h;

DOI:10.1080/10426500008045006

Reference yield: 78.0%

4-methoxy-benzaldehyde (123-11-5) + 2-(2-hydrazono-4-oxo-thiazolidin-3-yl)-6-(4-nitrophenylthio)benzthiazole (296232-32-1) → 2-{[1-(4-Methoxy-phenyl)-meth-(E)-ylidene]-hydrazono}-3-[6-(4-nitro-phenylsulfanyl)-benzothiazol-2-yl]-thiazolidin-4-one (296232-46-7)

Guidance literature:

With piperidine; In ethanol; Heating;

DOI:10.1080/10426500008045006

Reference yield: 75.0%

4-chlorobenzaldehyde (104-88-1) + 2-(2-hydrazono-4-oxo-thiazolidin-3-yl)-6-(4-nitrophenylthio)benzthiazole (296232-32-1) → 2-{[1-(4-Chloro-phenyl)-meth-(E)-ylidene]-hydrazono}-3-[6-(4-nitro-phenylsulfanyl)-benzothiazol-2-yl]-thiazolidin-4-one (296232-47-8)

Guidance literature:

With piperidine; In ethanol; Heating;

DOI:10.1080/10426500008045006

upstream raw materials:

2-(2'-thioxo-4'-oxo-thiazolidin-3'-yl)-6-(p-nitrophenylthio)benzthiazole

Downstream raw materials:

2-{[1-(4-Chloro-phenyl)-meth-(E)-ylidene]-hydrazono}-3-[6-(4-nitro-phenylsulfanyl)-benzothiazol-2-yl]-thiazolidin-4-one

3-[6-(4-Nitro-phenylsulfanyl)-benzothiazol-2-yl]-2-{[1-phenyl-meth-(E)-ylidene]-hydrazono}-thiazolidin-4-one

2-{[1-(4-Methoxy-phenyl)-meth-(E)-ylidene]-hydrazono}-3-[6-(4-nitro-phenylsulfanyl)-benzothiazol-2-yl]-thiazolidin-4-one

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