N-(3,5-dimethylphenyl)cyclohexylamine

Base Information

Chemical Name:N-(3,5-dimethylphenyl)cyclohexylamine
CAS No.:13342-30-8
Molecular Formula:C₁₄H₂₁N
Molecular Weight:203.327
Hs Code.:

Synonyms:N-(3,5-dimethylphenyl)cyclohexylamine

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Chemical Property of N-(3,5-dimethylphenyl)cyclohexylamine

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Technology Process of N-(3,5-dimethylphenyl)cyclohexylamine

There total 4 articles about N-(3,5-dimethylphenyl)cyclohexylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 556-96-7
5-bromo-1,3-xylene

: 108-91-8,157973-60-9
cyclohexylamine

: 13342-30-8
N-(3,5-dimethylphenyl)cyclohexylamine

Guidance literature:: With C₆₀H₈₆O₄P₂Pd₂⁽²⁺⁾*2BF₄^(1-); sodium t-butanolate; In 1,4-dioxane; at 100 ℃; for 3h;
DOI:10.1039/c8dt00119g

Reference yield:

: 108-91-8,157973-60-9
cyclohexylamine

: 325142-93-6
2-(3,5-dimethylphenyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

: 13342-30-8
N-(3,5-dimethylphenyl)cyclohexylamine

Guidance literature:: With potassium fluoride; 4 A molecular sieve; oxygen; copper diacetate; In acetonitrile; at 80 ℃; for 24h;
DOI:10.1021/ol062902w

Reference yield:

: 108-38-3,104809-90-7
m-xylene

: 13342-30-8
N-(3,5-dimethylphenyl)cyclohexylamine

Guidance literature:: Multi-step reaction with 2 steps

1: 4,4'-di-tert-butyl-2,2'-bipyridine; pinacolborane / [(COD)Ir(OMe)]2 / cyclohexane / 24 h / 80 °C

2: 83 mg / oxygen; potassium fluoride; molecular sieves 4 Angstroem / copper(II) acetate monohydrate / acetonitrile / 24 h / 80 °C

With potassium fluoride; pinacol borane; 4 A molecular sieve; oxygen; 4,4'-di-tert-butyl-2,2'-bipyridine; (1,5-cyclooctadiene)(methoxy)iridium(l) dimer; copper diacetate; In cyclohexane; acetonitrile;
DOI:10.1021/ol062902w