2,2'-dithiobis

Base Information

Chemical Name:2,2'-dithiobis
CAS No.:104857-38-7
Molecular Formula:C₂₆H₂₂N₄O₄S₂
Molecular Weight:518.617
Hs Code.:

2,2'-dithiobis<N-(4-methoxyphenyl)-3-pyridinecarboxamide>

Synonyms:2,2'-dithiobis

Suppliers and Price of 2,2'-dithiobis

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2,2'-dithiobis

Chemical Property:

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Technology Process of 2,2'-dithiobis

There total 3 articles about 2,2'-dithiobis which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2942-59-8
2-chloronicotinic acid

: 104857-38-7
2,2'-dithiobis

Guidance literature:: Multi-step reaction with 2 steps

1: 85 percent / thiourea / H₂O / 4 h / Heating

2: 1) thionyl chloride, pyridine / 1) CHCl₃, reflux, 1 h; 2) toluene, reflux, 1.5 h

With pyridine; thionyl chloride; thiourea; In water;
DOI:10.1002/jhet.5570220543

Reference yield:

: 27916-10-5
2,2'-dithiobis(3-pyridinecarboxylic acid)

: 104857-38-7
2,2'-dithiobis

Guidance literature:: Multi-step reaction with 2 steps

1: 90 percent / sodium bisulfite, 1M hydrochloric acid / 1 h / Ambient temperature

2: 1) thionyl chloride, pyridine / 1) CHCl₃, reflux, 1 h; 2) toluene, reflux, 1.5 h

With pyridine; hydrogenchloride; thionyl chloride; sodium hydrogensulfite;
DOI:10.1002/jhet.5570220543

Reference yield:

: 38521-46-9
1,2-dihydro-2-thioxo-3-pyridine carboxylic scid

: 104-94-9
4-methoxy-aniline

: 104857-38-7
2,2'-dithiobis

Guidance literature:: With pyridine; thionyl chloride; Yield given. Multistep reaction; 1) CHCl₃, reflux, 1 h; 2) toluene, reflux, 1.5 h;
DOI:10.1002/jhet.5570220543