Methyl 2-Dimethoxymethyl-1,3-dimethyl-4-oxocyclohex-2-enyl-1-carboxylat

Base Information

• Chemical Name: Methyl 2-Dimethoxymethyl-1,3-dimethyl-4-oxocyclohex-2-enyl-1-carboxylat
• CAS No.: 60705-22-8
• Molecular Formula: C₁₃H₂₀O₅
• Molecular Weight: 256.299
• Mol file: 60705-22-8.mol

Synonyms:Methyl 2-Dimethoxymethyl-1,3-dimethyl-4-oxocyclohex-2-enyl-1-carboxylat

Chemical Property of Methyl 2-Dimethoxymethyl-1,3-dimethyl-4-oxocyclohex-2-enyl-1-carboxylat

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Methyl 2-Dimethoxymethyl-1,3-dimethyl-4-oxocyclohex-2-enyl-1-carboxylat

There total 3 articles about Methyl 2-Dimethoxymethyl-1,3-dimethyl-4-oxocyclohex-2-enyl-1-carboxylat which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

Pyruvic aldehyde dimethyl acetal (6342-56-9) → Methyl 2-Dimethoxymethyl-1,3-dimethyl-4-oxocyclohex-2-enyl-1-carboxylat (60705-22-8)

Guidance literature:

Multi-step reaction with 3 steps

1: (i) NaH, (ii) /BRN= 1560557/

2: (i) NaH, (ii) /BRN= 969135/

3: NaOMe

With sodium methylate;

DOI:10.1021/jo00423a028

Reference yield:

4,4-dimethoxy-3-oxo-butyric acid methyl ester (60705-25-1) → Methyl 2-Dimethoxymethyl-1,3-dimethyl-4-oxocyclohex-2-enyl-1-carboxylat (60705-22-8)

Guidance literature:

Multi-step reaction with 2 steps

1: (i) NaH, (ii) /BRN= 969135/

2: NaOMe

With sodium methylate;

DOI:10.1021/jo00423a028

Reference yield:

4-penten-3-one (1629-58-9) + methyl 4,4-dimethoxy-2-methyl-3-oxobutanoate (119368-63-7) → Methyl 2-Dimethoxymethyl-1,3-dimethyl-4-oxocyclohex-2-enyl-1-carboxylat (60705-22-8)

Guidance literature:

With sodium methylate;

DOI:10.1021/jo00423a028

upstream raw materials:

4-penten-3-one

methyl 4,4-dimethoxy-2-methyl-3-oxobutanoate

Pyruvic aldehyde dimethyl acetal

4,4-dimethoxy-3-oxo-butyric acid methyl ester

Downstream raw materials:

7-E,9-E methyl trisporate B

Methyl 1,3-Dimethyl-2-formyl-4-oxocyclohex-2-enyl-1-carboxylat