C₄₅H₅₄N₅O₁₀⁽¹⁺⁾*NO₃^(1-)

Base Information

• Chemical Name: C₄₅H₅₄N₅O₁₀⁽¹⁺⁾*NO₃^(1-)
• CAS No.: 1619906-89-6
• Molecular Formula: C₄₅H₅₄N₅O₁₀*NO₃
• Molecular Weight: 886.956

Synonyms:C₄₅H₅₄N₅O₁₀⁽¹⁺⁾*NO₃^(1-)

Chemical Property of C₄₅H₅₄N₅O₁₀⁽¹⁺⁾*NO₃^(1-)

Chemical Property:

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Technology Process of C₄₅H₅₄N₅O₁₀⁽¹⁺⁾*NO₃^(1-)

There total 10 articles about C₄₅H₅₄N₅O₁₀⁽¹⁺⁾*NO₃^(1-) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

C45H54N5O10(1+)*I(1-) (1619906-93-2) → C45H54N5O10(1+)*NO3(1-) (1619906-89-6)

Guidance literature:

With nitrate loaded Amberlite column; In water; acetone;

DOI:10.1039/c4cc03200d

Reference yield:

2-{4-[2-(allyloxy)ethoxy]phenoxy}ethylamine (807326-89-2) → C45H54N5O10(1+)*NO3(1-) (1619906-89-6)

Guidance literature:

Multi-step reaction with 5 steps

1: dmap; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine / dichloromethane / 48 h / Inert atmosphere

2: potassium hydroxide / methanol / 16 h / Inert atmosphere

3: dmap; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane; N,N-dimethyl-formamide / 168 h / Inert atmosphere

4: N,N-dimethyl-formamide / 16 h / Inert atmosphere

5: nitrate loaded Amberlite? column / acetone; water

With dmap; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; potassium hydroxide; In methanol; dichloromethane; water; N,N-dimethyl-formamide; acetone;

DOI:10.1039/c4cc03200d

Reference yield:

pyridine-3,5-dicarboxylic acid monomethyl ester (5027-65-6) → C45H54N5O10(1+)*NO3(1-) (1619906-89-6)

Guidance literature:

Multi-step reaction with 5 steps

1: dmap; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine / dichloromethane / 48 h / Inert atmosphere

2: potassium hydroxide / methanol / 16 h / Inert atmosphere

3: dmap; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane; N,N-dimethyl-formamide / 168 h / Inert atmosphere

4: N,N-dimethyl-formamide / 16 h / Inert atmosphere

5: nitrate loaded Amberlite? column / acetone; water

With dmap; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; potassium hydroxide; In methanol; dichloromethane; water; N,N-dimethyl-formamide; acetone;

DOI:10.1039/c4cc03200d

upstream raw materials:

C₂₄H₃₁N₃O₅*C₂HF₃O₂

2-{4-[2-(allyloxy)ethoxy]phenoxy}ethylamine

C₄₅H₅₄N₅O₁₀⁽¹⁺⁾*I^(1-)

benzene 1,3-dicarboxylic acid monomethyl ester

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