methyl (2E)-2-{[N-(2-formylphenyl)(2-methylbenzene)sulfonamido]methyl}-3-(4-methylphenyl)prop-2-enoate

Base Information

Chemical Name:methyl (2E)-2-{[N-(2-formylphenyl)(2-methylbenzene)sulfonamido]methyl}-3-(4-methylphenyl)prop-2-enoate
CAS No.:1589493-37-7
Molecular Formula:C₂₆H₂₅NO₅S
Molecular Weight:463.554
Hs Code.:

Synonyms:methyl (2E)-2-{[N-(2-formylphenyl)(2-methylbenzene)sulfonamido]methyl}-3-(4-methylphenyl)prop-2-enoate

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Chemical Property of methyl (2E)-2-{[N-(2-formylphenyl)(2-methylbenzene)sulfonamido]methyl}-3-(4-methylphenyl)prop-2-enoate

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Technology Process of methyl (2E)-2-{[N-(2-formylphenyl)(2-methylbenzene)sulfonamido]methyl}-3-(4-methylphenyl)prop-2-enoate

There total 3 articles about methyl (2E)-2-{[N-(2-formylphenyl)(2-methylbenzene)sulfonamido]methyl}-3-(4-methylphenyl)prop-2-enoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 6590-65-4
N-(2-Formyl-phenyl)-4-methyl-benzenesulfonamide

: 213999-86-1
methyl (2Z)-2-(bromomethyl)-3-(2-methylphenyl)prop-2-enoate

: 1589493-37-7
methyl (2E)-2-{[N-(2-formylphenyl)(2-methylbenzene)sulfonamido]methyl}-3-(4-methylphenyl)prop-2-enoate

Guidance literature:: N-(2-Formyl-phenyl)-4-methyl-benzenesulfonamide; With potassium carbonate; In acetonitrile; at 20 ℃; for 0.25h;

methyl (2Z)-2-(bromomethyl)-3-(2-methylphenyl)prop-2-enoate; In acetonitrile; at 20 ℃; for 3h;
DOI:10.1039/c5ob01060h

Reference yield:

: 316807-89-3
2-(hydroxy-o-tolyl-methyl)-acrylic acid methyl ester

: 1589493-37-7
methyl (2E)-2-{[N-(2-formylphenyl)(2-methylbenzene)sulfonamido]methyl}-3-(4-methylphenyl)prop-2-enoate

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogen bromide; sulfuric acid / dichloromethane / 12 h / 0 - 20 °C

2: potassium carbonate / acetonitrile / 20 °C

With sulfuric acid; hydrogen bromide; potassium carbonate; In dichloromethane; acetonitrile;
DOI:10.1002/ejoc.201301422

Reference yield:

: 90312-02-0
N-(2-hydroxymethylphenyl)-4-methylbenzenesulfonamide

: 1589493-37-7
methyl (2E)-2-{[N-(2-formylphenyl)(2-methylbenzene)sulfonamido]methyl}-3-(4-methylphenyl)prop-2-enoate

Guidance literature:: Multi-step reaction with 2 steps

1.1: manganese(IV) oxide

2.1: potassium carbonate / acetonitrile / 0.25 h / 20 °C

2.2: 3 h / 20 °C

With manganese(IV) oxide; potassium carbonate; In acetonitrile;
DOI:10.1039/c5ob01060h