meso-N,N'-bis-(2,4,6-triisopropyl)phenylsulfonyl-1,2-diamino-1,2-diphenylethane

Base Information

Chemical Name:meso-N,N'-bis-(2,4,6-triisopropyl)phenylsulfonyl-1,2-diamino-1,2-diphenylethane
CAS No.:786712-30-9
Molecular Formula:C₄₄H₆₀N₂O₄S₂
Molecular Weight:745.103
Hs Code.:

Synonyms:meso-N,N'-bis-(2,4,6-triisopropyl)phenylsulfonyl-1,2-diamino-1,2-diphenylethane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of meso-N,N'-bis-(2,4,6-triisopropyl)phenylsulfonyl-1,2-diamino-1,2-diphenylethane

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Technology Process of meso-N,N'-bis-(2,4,6-triisopropyl)phenylsulfonyl-1,2-diamino-1,2-diphenylethane

There total 1 articles about meso-N,N'-bis-(2,4,6-triisopropyl)phenylsulfonyl-1,2-diamino-1,2-diphenylethane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 6553-96-4
2,4,6-triisopropylphenylsulfonyl chloride

: 951-87-1,5700-60-7,16635-95-3,29841-69-8,35132-20-8,107133-00-6
meso-1,2-diphenyl-1,2-diaminoethane

: 786712-30-9
meso-N,N'-bis-(2,4,6-triisopropyl)phenylsulfonyl-1,2-diamino-1,2-diphenylethane

Guidance literature:: With triethylamine; In tetrahydrofuran; at 80 ℃; for 15h;
DOI:10.1021/ol048498n

Reference yield: 65.0%

: 591-87-7
Allyl acetate

: 786712-30-9
meso-N,N'-bis-(2,4,6-triisopropyl)phenylsulfonyl-1,2-diamino-1,2-diphenylethane

: (1R,2S)-1-N-allyl-N,N'-bis-(2,4,6-triisopropyl)phenylsulfonyl-1,2-diamino-1,2-diphenylethane

Guidance literature:: With bis(η3-allyl-μ-chloropalladium(II)); chiral 1,2-diaminocyclohexane based Trost ligand; potassium tert-butylate; In dichloromethane; at -15 - 4 ℃; for 23h;
DOI:10.1021/jo052488y

Reference yield:

: 591-87-7
Allyl acetate

: 786712-30-9
meso-N,N'-bis-(2,4,6-triisopropyl)phenylsulfonyl-1,2-diamino-1,2-diphenylethane

: (1R,2S)-1-N-allyl-N,N'-bis-(2,4,6-triisopropyl)phenylsulfonyl-1,2-diamino-1,2-diphenylethane

: (1S,2R)-1-N-allyl-N,N'-bis-(2,4,6-triisopropyl)phenylsulfonyl-1,2-diamino-1,2-diphenylethane

Guidance literature:: With bis(η3-allyl-μ-chloropalladium(II)); potassium tert-butylate; (1R,2R)-1,2-bis[(2-diphenylphosphanyl)benzoylamino]cyclohexane; In 1,4-dioxane; toluene; at -15 - 0 ℃; for 23h; Title compound not separated from byproducts;
DOI:10.1021/ol048498n