4-methyl-2-p-tolylsulphonyl-2,3-dihydro-1,2-benzothiazepin-5(4H)-one

Base Information

• Chemical Name: 4-methyl-2-p-tolylsulphonyl-2,3-dihydro-1,2-benzothiazepin-5(4H)-one
• CAS No.: 74328-44-2
• Molecular Formula: C₁₇H₁₇NO₃S₂
• Molecular Weight: 347.459
• Mol file: 74328-44-2.mol

Synonyms:4-methyl-2-p-tolylsulphonyl-2,3-dihydro-1,2-benzothiazepin-5(4H)-one

Chemical Property of 4-methyl-2-p-tolylsulphonyl-2,3-dihydro-1,2-benzothiazepin-5(4H)-one

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 4-methyl-2-p-tolylsulphonyl-2,3-dihydro-1,2-benzothiazepin-5(4H)-one

There total 8 articles about 4-methyl-2-p-tolylsulphonyl-2,3-dihydro-1,2-benzothiazepin-5(4H)-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

2,2-dimethyl-1-p-tolylsulphonyliminobenzothiophen-3(2H)-one (74328-46-4) → 4-methyl-2-p-tolylsulphonyl-2,3-dihydro-1,2-benzothiazepin-5(4H)-one (74328-44-2)

Guidance literature:

With triethylamine; In benzene; Heating;

DOI:10.1016/S0040-4039(01)85548-9

Reference yield: 100.0%

3-methyl-1-(p-tolylsulphonylimino)thiochroman-4-one (74328-43-1) → 4-methyl-2-p-tolylsulphonyl-2,3-dihydro-1,2-benzothiazepin-5(4H)-one (74328-44-2)

Guidance literature:

With triethylamine; In chloroform; Ambient temperature;

DOI:10.1016/S0040-4039(01)85548-9

Reference yield: 100.0%

4-Methyl-N-[2-(2-methyl-acryloyl)-phenylsulfanyl]-benzenesulfonamide (76664-73-8) → 4-methyl-2-p-tolylsulphonyl-2,3-dihydro-1,2-benzothiazepin-5(4H)-one (74328-44-2)

Guidance literature:

With triethylamine; In chloroform; for 1h; Ambient temperature;

upstream raw materials:

3-methyl-2,3-dihydro-4H-thiochromen-4-one

chloroamine-T

4-Methyl-N-[2-(2-methyl-acryloyl)-phenylsulfanyl]-benzenesulfonamide

2,2-dimethyl-1-p-tolylsulphonyliminobenzothiophen-3(2H)-one

Downstream raw materials:

4-methyl-5-oxo-2-p-tolylsulphonyl-2,3,4,5-tetrahydro-1,2-benzothiazepine 1-oxide

4-methyl-5-oxo-2-p-tolylsulphonyl-2,3,4,5-tetrahydro-1,2-benzothiazepine 1,1-dioxide