Technology Process of C21H26OS2Si
There total 1 articles about C21H26OS2Si which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
bis(η3-allyl-μ-chloropalladium(II)); triphenyl-arsane; caesium carbonate;
In
1,4-dioxane; water;
at 90 ℃;
for 12h;
Inert atmosphere;
DOI:10.1016/j.tetlet.2012.04.059
- Guidance literature:
-
Multi-step reaction with 3 steps
1: water; toluene-4-sulfonic acid / acetone / 8 h / 20 °C / Inert atmosphere
2: bis(η3-allyl-μ-chloropalladium(II)); triphenyl-arsane; caesium carbonate / 1,4-dioxane; water / 12 h / 90 °C / Inert atmosphere
3: water; acetic acid / 1 h / 150 °C / Microwave irradiation
With
bis(η3-allyl-μ-chloropalladium(II)); triphenyl-arsane; water; caesium carbonate; toluene-4-sulfonic acid; acetic acid;
In
1,4-dioxane; water; acetone;
DOI:10.1016/j.tetlet.2012.04.059
- Guidance literature:
-
Multi-step reaction with 5 steps
1: water; toluene-4-sulfonic acid / acetone / 8 h / 20 °C / Inert atmosphere
2: bis(η3-allyl-μ-chloropalladium(II)); triphenyl-arsane; caesium carbonate / 1,4-dioxane; water / 12 h / 90 °C / Inert atmosphere
3: water; acetic acid / 1 h / 150 °C / Microwave irradiation
4: ammonium acetate / water / 12 h / 70 °C
5: trifluoroacetic acid / dichloromethane / 2 h / 20 °C / Inert atmosphere
With
bis(η3-allyl-μ-chloropalladium(II)); triphenyl-arsane; ammonium acetate; water; caesium carbonate; toluene-4-sulfonic acid; acetic acid; trifluoroacetic acid;
In
1,4-dioxane; dichloromethane; water; acetone;
4: Knoevenagel condensation;
DOI:10.1016/j.tetlet.2012.04.059
