2-methyl-(benzyl 5-azido-2,3,5-trideoxy-β-D-ribofuranosido)-<2,3-d>-2-oxazoline

Base Information

Chemical Name:2-methyl-(benzyl 5-azido-2,3,5-trideoxy-β-D-ribofuranosido)-<2,3-d>-2-oxazoline
CAS No.:74590-63-9
Molecular Formula:C₁₄H₁₆N₄O₃
Molecular Weight:288.306
Hs Code.:

Synonyms:2-methyl-(benzyl 5-azido-2,3,5-trideoxy-β-D-ribofuranosido)-<2,3-d>-2-oxazoline

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Chemical Property of 2-methyl-(benzyl 5-azido-2,3,5-trideoxy-β-D-ribofuranosido)-<2,3-d>-2-oxazoline

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Technology Process of 2-methyl-(benzyl 5-azido-2,3,5-trideoxy-β-D-ribofuranosido)-<2,3-d>-2-oxazoline

There total 6 articles about 2-methyl-(benzyl 5-azido-2,3,5-trideoxy-β-D-ribofuranosido)-<2,3-d>-2-oxazoline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 66166-90-3
benzyl 2-(benzyloxycarbonylamino)-2-deoxy-β-D-xylofuranoside

: 74590-63-9
2-methyl-(benzyl 5-azido-2,3,5-trideoxy-β-D-ribofuranosido)-<2,3-d>-2-oxazoline

Guidance literature:: Multi-step reaction with 3 steps

1: 85 percent / pyridine / 3 h / 0 °C

2: 1.) hydrogen / 1.) 10percent Pd-C / 1.) 1,4-dioxane/methanol, room temperature, 2.5 h; 2.)methanol, room temperature, 30 min

3: 1.) sodium azide / 1.) N,N-dimethylformamide, 90 degC; 2.) N,N-dimethylformamide, 90 degC

With pyridine; sodium azide; hydrogen; palladium on activated charcoal;
DOI:10.1016/S0008-6215(00)85674-8

Reference yield:

: 74593-10-5
benzyl 2-(benzyloxycarbonylamino)-2-deoxy-3,5-di-O-mesyl-β-D-xylofuranoside

: 74590-63-9
2-methyl-(benzyl 5-azido-2,3,5-trideoxy-β-D-ribofuranosido)-<2,3-d>-2-oxazoline

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) hydrogen / 1.) 10percent Pd-C / 1.) 1,4-dioxane/methanol, room temperature, 2.5 h; 2.)methanol, room temperature, 30 min

2: 1.) sodium azide / 1.) N,N-dimethylformamide, 90 degC; 2.) N,N-dimethylformamide, 90 degC

With sodium azide; hydrogen; palladium on activated charcoal;
DOI:10.1016/S0008-6215(00)85674-8

Reference yield:

: 74593-13-8
benzyl 2-acetamido-2-deoxy-3,5-di-O-mesyl-β-D-xylofuranoside

: 74590-63-9
2-methyl-(benzyl 5-azido-2,3,5-trideoxy-β-D-ribofuranosido)-<2,3-d>-2-oxazoline

Guidance literature:: With sodium azide; Yield given. Multistep reaction; 1.) N,N-dimethylformamide, 90 degC; 2.) N,N-dimethylformamide, 90 degC;
DOI:10.1016/S0008-6215(00)85674-8