(R)-2-Propyl-2H-pyridine-1-carboxylic acid (1R,2S,5R)-5-methyl-2-[1-methyl-1-(4-phenoxy-phenyl)-ethyl]-cyclohexyl ester

Base Information

• Chemical Name: (R)-2-Propyl-2H-pyridine-1-carboxylic acid (1R,2S,5R)-5-methyl-2-[1-methyl-1-(4-phenoxy-phenyl)-ethyl]-cyclohexyl ester
• CAS No.: 137769-35-8
• Molecular Formula: C₃₁H₃₉NO₃
• Molecular Weight: 473.656

Synonyms:(R)-2-Propyl-2H-pyridine-1-carboxylic acid (1R,2S,5R)-5-methyl-2-[1-methyl-1-(4-phenoxy-phenyl)-ethyl]-cyclohexyl ester

Chemical Property of (R)-2-Propyl-2H-pyridine-1-carboxylic acid (1R,2S,5R)-5-methyl-2-[1-methyl-1-(4-phenoxy-phenyl)-ethyl]-cyclohexyl ester

Chemical Property:

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Technology Process of (R)-2-Propyl-2H-pyridine-1-carboxylic acid (1R,2S,5R)-5-methyl-2-[1-methyl-1-(4-phenoxy-phenyl)-ethyl]-cyclohexyl ester

There total 2 articles about (R)-2-Propyl-2H-pyridine-1-carboxylic acid (1R,2S,5R)-5-methyl-2-[1-methyl-1-(4-phenoxy-phenyl)-ethyl]-cyclohexyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-propylmagnesium chloride (2234-82-4) + 3-(triisopropylstannyl)pyridine (137769-42-7) + (1R,2S,5R)-8-(4-phenoxyphenyl)menthyl chloroformate (137769-43-8) → (R)-2-Propyl-2H-pyridine-1-carboxylic acid (1R,2S,5R)-5-methyl-2-[1-methyl-1-(4-phenoxy-phenyl)-ethyl]-cyclohexyl ester (137769-35-8) + (S)-2-Propyl-2H-pyridine-1-carboxylic acid (1R,2S,5R)-5-methyl-2-[1-methyl-1-(4-phenoxy-phenyl)-ethyl]-cyclohexyl ester (137769-35-8)

Guidance literature:

Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts;

DOI:10.1021/jo00026a004

Reference yield:

1-propylmagnesium chloride (2234-82-4) + 3-(triisopropylstannyl)pyridine (137769-42-7) + (1R,2S,5R)-8-(4-phenoxyphenyl)menthyl chloroformate (137769-43-8) → (R)-2-Propyl-2H-pyridine-1-carboxylic acid (1R,2S,5R)-5-methyl-2-[1-methyl-1-(4-phenoxy-phenyl)-ethyl]-cyclohexyl ester (137769-35-8) + (S)-2-Propyl-2H-pyridine-1-carboxylic acid (1R,2S,5R)-5-methyl-2-[1-methyl-1-(4-phenoxy-phenyl)-ethyl]-cyclohexyl ester (137769-35-8)

Guidance literature:

Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts;

DOI:10.1021/jo00026a004

Reference yield: 89.0%

(R)-2-Propyl-2H-pyridine-1-carboxylic acid (1R,2S,5R)-5-methyl-2-[1-methyl-1-(4-phenoxy-phenyl)-ethyl]-cyclohexyl ester (137769-35-8) → (R)-2-Propyl-piperidine-1-carboxylic acid (1R,2S,5R)-5-methyl-2-[1-methyl-1-(4-phenoxy-phenyl)-ethyl]-cyclohexyl ester (137769-50-7)

Guidance literature:

With hydrogen; platinum(IV) oxide;

DOI:10.1021/jo00026a004

upstream raw materials:

1-propylmagnesium chloride

3-(triisopropylstannyl)pyridine

(1R,2S,5R)-8-(4-phenoxyphenyl)menthyl chloroformate

Downstream raw materials:

(R)-2-Propyl-piperidine-1-carboxylic acid (1R,2S,5R)-5-methyl-2-[1-methyl-1-(4-phenoxy-phenyl)-ethyl]-cyclohexyl ester

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