N-(7-chloro-2-methylquinolin-4-yl)-N-(3-((diethylamino)methyl)-4-hydroxyphenyl)-2,3-dichlorobenzenesulfonamide

Base Information

Chemical Name:N-(7-chloro-2-methylquinolin-4-yl)-N-(3-((diethylamino)methyl)-4-hydroxyphenyl)-2,3-dichlorobenzenesulfonamide
CAS No.:1417177-53-7
Molecular Formula:C₂₇H₂₆Cl₃N₃O₃S
Molecular Weight:578.947
Hs Code.:

Synonyms:N-(7-chloro-2-methylquinolin-4-yl)-N-(3-((diethylamino)methyl)-4-hydroxyphenyl)-2,3-dichlorobenzenesulfonamide

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Chemical Property of N-(7-chloro-2-methylquinolin-4-yl)-N-(3-((diethylamino)methyl)-4-hydroxyphenyl)-2,3-dichlorobenzenesulfonamide

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Technology Process of N-(7-chloro-2-methylquinolin-4-yl)-N-(3-((diethylamino)methyl)-4-hydroxyphenyl)-2,3-dichlorobenzenesulfonamide

There total 8 articles about N-(7-chloro-2-methylquinolin-4-yl)-N-(3-((diethylamino)methyl)-4-hydroxyphenyl)-2,3-dichlorobenzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 102374-64-1
4-(7-chloro-2-methylquinolin-4-ylamino)-2-((diethylamino)methyl)phenol

: 82417-45-6
dichlorobenzenesulfonyl chloride

: 1417177-53-7
N-(7-chloro-2-methylquinolin-4-yl)-N-(3-((diethylamino)methyl)-4-hydroxyphenyl)-2,3-dichlorobenzenesulfonamide

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In acetone; for 3.5h; Inert atmosphere;

Reference yield:

: 15644-88-9
7-chloro-4-hydroxy-2-methylquinoline

: 1417177-53-7
N-(7-chloro-2-methylquinolin-4-yl)-N-(3-((diethylamino)methyl)-4-hydroxyphenyl)-2,3-dichlorobenzenesulfonamide

Guidance literature:: Multi-step reaction with 3 steps

1.1: trichlorophosphate / 2.5 h / 120 °C

2.1: hydrogenchloride; water / 2 h / Reflux

2.2: 6 h / Reflux

3.1: N-ethyl-N,N-diisopropylamine / acetone / 3.5 h / Inert atmosphere

With hydrogenchloride; water; N-ethyl-N,N-diisopropylamine; trichlorophosphate; In acetone;

Reference yield:

: 108-42-9
3-chloro-aniline

: 1417177-53-7
N-(7-chloro-2-methylquinolin-4-yl)-N-(3-((diethylamino)methyl)-4-hydroxyphenyl)-2,3-dichlorobenzenesulfonamide

Guidance literature:: Multi-step reaction with 4 steps

1.1: hydrogenchloride / 25 °C

2.1: trichlorophosphate / 2.5 h / 120 °C

3.1: hydrogenchloride; water / 2 h / Reflux

3.2: 6 h / Reflux

4.1: N-ethyl-N,N-diisopropylamine / acetone / 3.5 h / Inert atmosphere

With hydrogenchloride; water; N-ethyl-N,N-diisopropylamine; trichlorophosphate; In acetone;