2-[2-(diphenylphosphorothioyl)ethyl]tellanylethyl(diphenyl)phosphine sulfide

Base Information

Chemical Name:2-[2-(diphenylphosphorothioyl)ethyl]tellanylethyl(diphenyl)phosphine sulfide
CAS No.:1357196-43-0
Molecular Formula:C₂₈H₂₈P₂S₂Te
Molecular Weight:618.21
Hs Code.:

Synonyms:2-[2-(diphenylphosphorothioyl)ethyl]tellanylethyl(diphenyl)phosphine sulfide

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Chemical Property of 2-[2-(diphenylphosphorothioyl)ethyl]tellanylethyl(diphenyl)phosphine sulfide

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Technology Process of 2-[2-(diphenylphosphorothioyl)ethyl]tellanylethyl(diphenyl)phosphine sulfide

There total 2 articles about 2-[2-(diphenylphosphorothioyl)ethyl]tellanylethyl(diphenyl)phosphine sulfide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 63000-06-6
divinyltellane

: 6591-07-7
diphenylphosphane sulfide

: 1357196-44-1
diphenyl(2-(vinyltellanyl)ethyl)phosphine sulfide

: 1357196-43-0
2-[2-(diphenylphosphorothioyl)ethyl]tellanylethyl(diphenyl)phosphine sulfide

Guidance literature:: With 2,2'-azobis(isobutyronitrile); In tetrahydrofuran; at 63 - 68 ℃; regioselective reaction; Inert atmosphere;
DOI:10.1134/S1070363211120152

Reference yield:

: 829-85-6
diphenylphosphane

: 1357196-44-1
diphenyl(2-(vinyltellanyl)ethyl)phosphine sulfide

: 1357196-43-0
2-[2-(diphenylphosphorothioyl)ethyl]tellanylethyl(diphenyl)phosphine sulfide

Guidance literature:: Multi-step reaction with 2 steps

1: sulfur / ethanol / 20 °C

2: 2,2'-azobis(isobutyronitrile) / tetrahydrofuran / 2.5 h / 60 - 68 °C / Inert atmosphere

With 2,2'-azobis(isobutyronitrile); sulfur; In tetrahydrofuran; ethanol;
DOI:10.1016/j.jorganchem.2013.07.050