α-formylcaprylate

Base Information

Chemical Name:α-formylcaprylate
CAS No.:86654-32-2
Molecular Formula:C₁₀H₁₈O₃
Molecular Weight:186.251
Hs Code.:

Synonyms:α-formylcaprylate

Suppliers and Price of α-formylcaprylate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of α-formylcaprylate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of α-formylcaprylate

There total 1 articles about α-formylcaprylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 7367-81-9
methyl (E)-oct-2-enoate

: 201230-82-2
carbon monoxide

: 111-11-5
methyl octanate

: 86654-32-2
α-formylcaprylate

Guidance literature:: With hydrogen; acetylacetonatodicarbonylrhodium(l); In dichloromethane; at 25 ℃; for 24h; under 7500.75 Torr;
DOI:10.1002/anie.200800956

Reference yield:

: 86654-32-2
α-formylcaprylate

: 86654-34-4
6-Hexyl-2-oxo-3-phenylsulfanyl-2,4,5,6-tetrahydro-benzofuran-6-carboxylic acid methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: KF / dimethylsulfoxide; 1,2-dimethoxy-ethane / Ambient temperature

2: 90 percent / SOCl₂ / pyridine / 0 °C

With potassium fluoride; thionyl chloride; In pyridine; 1,2-dimethoxyethane; dimethyl sulfoxide;
DOI:10.1246/cl.1983.881

Reference yield:

: 81470-07-7
α-(phenylthio)-β-vinylbutenolide

: 86654-32-2
α-formylcaprylate

: 86654-33-3,86667-94-9
(6R,7R,7aS)-6-Hexyl-7-hydroxy-2-oxo-3-phenylsulfanyl-2,4,5,6,7,7a-hexahydro-benzofuran-6-carboxylic acid methyl ester

: 86654-33-3,86667-94-9
(6R,7S,7aR)-6-Hexyl-7-hydroxy-2-oxo-3-phenylsulfanyl-2,4,5,6,7,7a-hexahydro-benzofuran-6-carboxylic acid methyl ester

Guidance literature:: With potassium fluoride; In 1,2-dimethoxyethane; dimethyl sulfoxide; Yield given; Ambient temperature;
DOI:10.1246/cl.1983.881