1,1-dimethylethyl -<1-methyl-1-<1-(1-phenylethyl)-3-pyrrolidinyl>ethyl>carbamate

Base Information

Chemical Name:1,1-dimethylethyl -<1-methyl-1-<1-(1-phenylethyl)-3-pyrrolidinyl>ethyl>carbamate
CAS No.:153566-72-4
Molecular Formula:C₂₀H₃₂N₂O₂
Molecular Weight:332.486
Hs Code.:

1,1-dimethylethyl <S-(R*,R*)>-<1-methyl-1-<1-(1-phenylethyl)-3-pyrrolidinyl>ethyl>carbamate

Synonyms:1,1-dimethylethyl -<1-methyl-1-<1-(1-phenylethyl)-3-pyrrolidinyl>ethyl>carbamate

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Chemical Property of 1,1-dimethylethyl -<1-methyl-1-<1-(1-phenylethyl)-3-pyrrolidinyl>ethyl>carbamate

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Technology Process of 1,1-dimethylethyl -<1-methyl-1-<1-(1-phenylethyl)-3-pyrrolidinyl>ethyl>carbamate

There total 1 articles about 1,1-dimethylethyl -<1-methyl-1-<1-(1-phenylethyl)-3-pyrrolidinyl>ethyl>carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: -α,α-dimethyl-1-(1-phenylethyl)-3-pyrrolidineacetic acid

: 75-65-0
tert-butyl alcohol

: 153566-72-4
1,1-dimethylethyl -<1-methyl-1-<1-(1-phenylethyl)-3-pyrrolidinyl>ethyl>carbamate

Guidance literature:: With 3 A molecular sieve; diphenyl phosphoryl azide; triethylamine; Yield given. Multistep reaction; 1.) 1 h, 2.) reflux, 30 h;
DOI:10.1021/jm00032a005

Reference yield: 85.0%

: 153566-72-4
1,1-dimethylethyl -<1-methyl-1-<1-(1-phenylethyl)-3-pyrrolidinyl>ethyl>carbamate

: 139230-22-1
1,1-dimethylethyl (S)-<1-methyl-1-(3-pyrrolidinyl)ethyl>carbamate

Guidance literature:: With hydrogen; palladium on activated charcoal; In methanol; for 14h; under 2585.7 Torr;
DOI:10.1021/jm00032a005

Reference yield:

: 153566-72-4
1,1-dimethylethyl -<1-methyl-1-<1-(1-phenylethyl)-3-pyrrolidinyl>ethyl>carbamate

: 7-[(S)-3-(1-Amino-1-methyl-ethyl)-pyrrolidin-1-yl]-1-(2,4-difluoro-phenyl)-6-fluoro-4-oxo-1,4-dihydro-[1,8]naphthyridine-3-carboxylic acid; hydrochloride

Guidance literature:: Multi-step reaction with 3 steps

1: 85 percent / H₂ / 20percent Pd/C / methanol / 14 h / 2585.7 Torr

2: Et₃N / acetonitrile / 18 h / Heating

3: HCl (g) / CH₂Cl₂ / Ambient temperature

With hydrogenchloride; hydrogen; triethylamine; palladium on activated charcoal; In methanol; dichloromethane; acetonitrile;
DOI:10.1021/jm00032a005