cholest-5-en-3β-yl 6-<(p-carboxybenzyl)thio>hexyl ether succinimido ester

Base Information

Chemical Name:cholest-5-en-3β-yl 6-<(p-carboxybenzyl)thio>hexyl ether succinimido ester
CAS No.:103003-27-6
Molecular Formula:C₄₅H₆₇NO₅S
Molecular Weight:734.097
Hs Code.:

Synonyms:cholest-5-en-3β-yl 6-<(p-carboxybenzyl)thio>hexyl ether succinimido ester

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Chemical Property of cholest-5-en-3β-yl 6-<(p-carboxybenzyl)thio>hexyl ether succinimido ester

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Technology Process of cholest-5-en-3β-yl 6-<(p-carboxybenzyl)thio>hexyl ether succinimido ester

There total 9 articles about cholest-5-en-3β-yl 6-<(p-carboxybenzyl)thio>hexyl ether succinimido ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.6%

: 6066-82-6
1-hydroxy-pyrrolidine-2,5-dione

: 103003-26-5
cholest-5-en-3β-yl 6-<(p-carboxybenzyl)thio>hexyl ether

: 103003-27-6
cholest-5-en-3β-yl 6-<(p-carboxybenzyl)thio>hexyl ether succinimido ester

Guidance literature:: With dicyclohexyl-carbodiimide; In dichloromethane; at 0 ℃; for 2h;
DOI:10.1021/jm00160a004

Reference yield:

: 629-11-8
1,6-hexanediol

: 103003-27-6
cholest-5-en-3β-yl 6-<(p-carboxybenzyl)thio>hexyl ether succinimido ester

Guidance literature:: Multi-step reaction with 7 steps

1: dioxane

2: 85 percent / pyridine / 4 h / 25 °C

3: NaI / acetone

4: ethanol / 8 h / Heating

5: aq. NaOH / ethanol / 14 h / Heating

6: 51.6 percent / NaOMe / benzene; methanol / 0.75 h / Ambient temperature

7: 96.6 percent / dicyclohexylcarbodiimide / CH₂Cl₂ / 2 h / 0 °C

With pyridine; sodium hydroxide; sodium methylate; dicyclohexyl-carbodiimide; sodium iodide; In 1,4-dioxane; methanol; ethanol; dichloromethane; acetone; benzene;
DOI:10.1021/jm00160a004

Reference yield:

: 57-88-5
cholesterol

: 103003-27-6
cholest-5-en-3β-yl 6-<(p-carboxybenzyl)thio>hexyl ether succinimido ester

Guidance literature:: Multi-step reaction with 8 steps

1: pyridine

2: dioxane

3: 85 percent / pyridine / 4 h / 25 °C

4: NaI / acetone

5: ethanol / 8 h / Heating

6: aq. NaOH / ethanol / 14 h / Heating

7: 51.6 percent / NaOMe / benzene; methanol / 0.75 h / Ambient temperature

8: 96.6 percent / dicyclohexylcarbodiimide / CH₂Cl₂ / 2 h / 0 °C

With pyridine; sodium hydroxide; sodium methylate; dicyclohexyl-carbodiimide; sodium iodide; In 1,4-dioxane; methanol; ethanol; dichloromethane; acetone; benzene;
DOI:10.1021/jm00160a004