Technology Process of C22H23N3O6
There total 6 articles about C22H23N3O6 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
copper(ll) sulfate pentahydrate; sodium L-ascorbate;
In
tetrahydrofuran; methanol; water;
at 20 ℃;
for 12h;
Inert atmosphere;
DOI:10.1021/jo300063u
- Guidance literature:
-
Multi-step reaction with 2 steps
1: tetrabutyl ammonium fluoride / tetrahydrofuran / 0.08 h / 0 °C / Inert atmosphere
2: copper(ll) sulfate pentahydrate; sodium L-ascorbate / tetrahydrofuran; methanol; water / 12 h / 20 °C / Inert atmosphere
With
copper(ll) sulfate pentahydrate; tetrabutyl ammonium fluoride; sodium L-ascorbate;
In
tetrahydrofuran; methanol; water;
DOI:10.1021/jo300063u
- Guidance literature:
-
Multi-step reaction with 4 steps
1: potassium carbonate / N,N-dimethyl-formamide / 12 h / 20 °C / Inert atmosphere
2: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; triethylamine / tetrahydrofuran / 12 h / 20 °C / Inert atmosphere
3: tetrabutyl ammonium fluoride / tetrahydrofuran / 0.08 h / 0 °C / Inert atmosphere
4: copper(ll) sulfate pentahydrate; sodium L-ascorbate / tetrahydrofuran; methanol; water / 12 h / 20 °C / Inert atmosphere
With
bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; copper(ll) sulfate pentahydrate; tetrabutyl ammonium fluoride; potassium carbonate; sodium L-ascorbate; triethylamine;
In
tetrahydrofuran; methanol; water; N,N-dimethyl-formamide;
DOI:10.1021/jo300063u
