1,4-di-{[(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)dithio]methyl}benzene

Base Information

Chemical Name:1,4-di-{[(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)dithio]methyl}benzene
CAS No.:1379507-87-5
Molecular Formula:C₃₆H₄₆O₁₈S₄
Molecular Weight:895.014
Hs Code.:

Synonyms:1,4-di-{[(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)dithio]methyl}benzene

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Chemical Property of 1,4-di-{[(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)dithio]methyl}benzene

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Technology Process of 1,4-di-{[(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)dithio]methyl}benzene

There total 4 articles about 1,4-di-{[(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)dithio]methyl}benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 105-09-9
1,4-bis(mercaptomethyl)benzene

: 1379507-87-5
1,4-di-{[(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)dithio]methyl}benzene

Guidance literature:: Multi-step reaction with 3 steps

1: N-benzyl-trimethylammonium hydroxide / tetrahydrofuran / 1.83 h / -78 °C

2: 3-chloro-benzenecarboperoxoic acid / dichloromethane / -78 °C

3: 1,2-dichloro-ethane / 83 °C

With N-benzyl-trimethylammonium hydroxide; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; dichloromethane; 1,2-dichloro-ethane;
DOI:10.1016/j.bmc.2012.03.070

Reference yield:

: 19879-84-6
tetraacetyl thioglucose

: 1586047-32-6
1-{[(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)dithio]methyl}-4-{[(2-methoxycarbonylethyl)sulfinyl]methyl}benzene

: 1379507-87-5
1,4-di-{[(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)dithio]methyl}benzene

Guidance literature:: 1-{[(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)dithio]methyl}-4-{[(2-methoxycarbonylethyl)sulfinyl]methyl}benzene; In dichloromethane; at 80 ℃; Neutral conditions;

tetraacetyl thioglucose; In dichloromethane; Heating;
DOI:10.1080/17415993.2013.778259

Reference yield:

: 1379507-93-3
3,3'-[1,4-phenylenebis(sulfinyl)]bispropanoic acid 1,1'-dimethyl ester

: 1379507-87-5
1,4-di-{[(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)dithio]methyl}benzene

Guidance literature:: Multi-step reaction with 2 steps

1.1: dichloromethane / 83 °C

2.1: dichloromethane / 80 °C / Neutral conditions

2.2: Heating

In dichloromethane;
DOI:10.1080/17415993.2013.778259