[10-(tert-butyldimethylsilanyloxymethyl)-anthracen-9-ylmethyl]-[2-(5,5-dimethyl-[1,3,2]dioxaborinan-2-yl)-benzyl]-methylamine

Base Information

Chemical Name:[10-(tert-butyldimethylsilanyloxymethyl)-anthracen-9-ylmethyl]-[2-(5,5-dimethyl-[1,3,2]dioxaborinan-2-yl)-benzyl]-methylamine
CAS No.:247027-55-0
Molecular Formula:C₃₅H₄₆BNO₃Si
Molecular Weight:567.652
Hs Code.:

Synonyms:[10-(tert-butyldimethylsilanyloxymethyl)-anthracen-9-ylmethyl]-[2-(5,5-dimethyl-[1,3,2]dioxaborinan-2-yl)-benzyl]-methylamine

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Chemical Property of [10-(tert-butyldimethylsilanyloxymethyl)-anthracen-9-ylmethyl]-[2-(5,5-dimethyl-[1,3,2]dioxaborinan-2-yl)-benzyl]-methylamine

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Technology Process of [10-(tert-butyldimethylsilanyloxymethyl)-anthracen-9-ylmethyl]-[2-(5,5-dimethyl-[1,3,2]dioxaborinan-2-yl)-benzyl]-methylamine

There total 6 articles about [10-(tert-butyldimethylsilanyloxymethyl)-anthracen-9-ylmethyl]-[2-(5,5-dimethyl-[1,3,2]dioxaborinan-2-yl)-benzyl]-methylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 42.0%

: 166821-88-1
5,5-dimethyl-2-(2-bromomethylphenyl)-1,3,2-dioxaborinane

: 247027-52-7
[10-(tert-butyldimethylsilanyloxymethyl)-anthracen-9-ylmethyl]-methylamine

: 247027-55-0
[10-(tert-butyldimethylsilanyloxymethyl)-anthracen-9-ylmethyl]-[2-(5,5-dimethyl-[1,3,2]dioxaborinan-2-yl)-benzyl]-methylamine

Guidance literature:: With potassium carbonate; In acetonitrile; for 20h; Heating;
DOI:10.1006/bioo.2001.1219

Reference yield:

: 71774-88-4
10-hydroxymethyl-9-anthracenecarboxaldehyde

: 247027-55-0
[10-(tert-butyldimethylsilanyloxymethyl)-anthracen-9-ylmethyl]-[2-(5,5-dimethyl-[1,3,2]dioxaborinan-2-yl)-benzyl]-methylamine

Guidance literature:: Multi-step reaction with 4 steps

1: 91 percent / imidazole / dimethylformamide / 14 h / 20 °C

2: methanol / 6 h / 20 °C

3: 1.95 g / sodium borohydride / methanol / 2 h / 20 °C

4: 42 percent / potassium carbonate / acetonitrile / 20 h / Heating

With 1H-imidazole; sodium tetrahydroborate; potassium carbonate; In methanol; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1021/ol9908732

Reference yield:

: 247027-51-6
10-(tert-butyl-dimethyl-silanyloxymethyl)-anthracene-9-carbaldehyde

: 247027-55-0
[10-(tert-butyldimethylsilanyloxymethyl)-anthracen-9-ylmethyl]-[2-(5,5-dimethyl-[1,3,2]dioxaborinan-2-yl)-benzyl]-methylamine

Guidance literature:: Multi-step reaction with 3 steps

1: methanol / 6 h / 20 °C

2: 1.95 g / sodium borohydride / methanol / 2 h / 20 °C

3: 42 percent / potassium carbonate / acetonitrile / 20 h / Heating

With sodium tetrahydroborate; potassium carbonate; In methanol; acetonitrile;
DOI:10.1021/ol9908732