1-(Bromomethyl)-3,5-diethoxybenzene

Base Information

Chemical Name:1-(Bromomethyl)-3,5-diethoxybenzene
CAS No.:238405-74-8
Molecular Formula:C₁₁H₁₅BrO₂
Molecular Weight:259.143
Hs Code.:
DSSTox Substance ID:DTXSID60593620
Wikidata:Q82488133
Mol file:238405-74-8.mol

Synonyms:1-(BROMOMETHYL)-3,5-DIETHOXYBENZENE;238405-74-8;SCHEMBL2935967;DTXSID60593620

Suppliers and Price of 1-(Bromomethyl)-3,5-diethoxybenzene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Labseeker
1-(bromomethyl)-3,5-diethoxybenzene 95
10g
$ 2163.00

Labseeker
1-(bromomethyl)-3,5-diethoxybenzene 95
5g
$ 1467.00

American Custom Chemicals Corporation
1-(BROMOMETHYL)-3,5-DIETHOXYBENZENE 95.00%
5MG
$ 500.87

Total 1 raw suppliers

Chemical Property of 1-(Bromomethyl)-3,5-diethoxybenzene

Chemical Property:

Boiling Point:322.5±27.0 °C(Predicted)
Density:1.296±0.06 g/cm3(Predicted)
XLogP3:3.2
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:5
Exact Mass:258.02554
Heavy Atom Count:14
Complexity:138

Purity/Quality:: 1-(bromomethyl)-3,5-diethoxybenzene 95 ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CCOC1=CC(=CC(=C1)CBr)OCC

Technology Process of 1-(Bromomethyl)-3,5-diethoxybenzene

There total 2 articles about 1-(Bromomethyl)-3,5-diethoxybenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.4%

: 198623-56-2
3,5-diethoxybenzyl alcohol

: 238405-74-8
1-(bromomethyl)-3,5-diethoxybenzene

Guidance literature:: With pyridine; phosphorus tribromide; In dichloromethane; at 0 - 20 ℃; for 4h;
DOI:10.1016/j.tet.2016.05.073

Reference yield:

: 29654-55-5
5-(hydroxymethyl)benzene-1,3-diol

: 238405-74-8
1-(bromomethyl)-3,5-diethoxybenzene

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate / acetone / 18 h / Inert atmosphere; Reflux

2: phosphorus tribromide; pyridine / dichloromethane / 4 h / 0 - 20 °C

With pyridine; phosphorus tribromide; potassium carbonate; In dichloromethane; acetone;
DOI:10.1016/j.tet.2016.05.073