Technology Process of C31H40NO6P
There total 4 articles about C31H40NO6P which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
triethylamine;
In
dichloromethane;
at 20 ℃;
for 3h;
DOI:10.1021/jm2000085
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: potassium chloride; tetrabutylammonium acetate; palladium diacetate; potassium carbonate / N,N-dimethyl-formamide / 4 h / 90 °C
2.1: phenol / 6 h / 100 °C
2.2: 24 h / Reflux
3.1: pyridine; ethanol / 20 °C
3.2: 0.5 h / 20 °C
3.3: 2 h / 0 - 20 °C
4.1: triethylamine / dichloromethane / 3 h / 20 °C
With
potassium chloride; tetrabutylammonium acetate; palladium diacetate; potassium carbonate; triethylamine; phenol;
In
pyridine; ethanol; dichloromethane; N,N-dimethyl-formamide;
1.1: Mizoroki-Heck reaction;
DOI:10.1021/jm2000085
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: phenol / 6 h / 100 °C
1.2: 24 h / Reflux
2.1: pyridine; ethanol / 20 °C
2.2: 0.5 h / 20 °C
2.3: 2 h / 0 - 20 °C
3.1: triethylamine / dichloromethane / 3 h / 20 °C
With
triethylamine; phenol;
In
pyridine; ethanol; dichloromethane;
DOI:10.1021/jm2000085