2-O-benzyl-1,3-bis[(1,2-di-O-myristyl-sn-glycero-3)-phosphoryl]glycerol di(2-cyanoethyl) ester

Base Information

Chemical Name:2-O-benzyl-1,3-bis[(1,2-di-O-myristyl-sn-glycero-3)-phosphoryl]glycerol di(2-cyanoethyl) ester
CAS No.:680220-11-5
Molecular Formula:C₇₈H₁₄₆N₂O₁₃P₂
Molecular Weight:1381.97
Hs Code.:

Synonyms:2-O-benzyl-1,3-bis[(1,2-di-O-myristyl-sn-glycero-3)-phosphoryl]glycerol di(2-cyanoethyl) ester

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Chemical Property of 2-O-benzyl-1,3-bis[(1,2-di-O-myristyl-sn-glycero-3)-phosphoryl]glycerol di(2-cyanoethyl) ester

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Technology Process of 2-O-benzyl-1,3-bis[(1,2-di-O-myristyl-sn-glycero-3)-phosphoryl]glycerol di(2-cyanoethyl) ester

There total 2 articles about 2-O-benzyl-1,3-bis[(1,2-di-O-myristyl-sn-glycero-3)-phosphoryl]glycerol di(2-cyanoethyl) ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: Diisopropyl-phosphoramidous acid (R)-2,3-bis-tetradecyloxy-propyl ester 2-cyano-ethyl ester

: 14690-00-7
2-O-benzylglycerol

: 680220-11-5
2-O-benzyl-1,3-bis[(1,2-di-O-myristyl-sn-glycero-3)-phosphoryl]glycerol di(2-cyanoethyl) ester

Guidance literature:: Diisopropyl-phosphoramidous acid (R)-2,3-bis-tetradecyloxy-propyl ester 2-cyano-ethyl ester; 2-O-benzylglycerol; With 1H-tetrazole; In dichloromethane; acetonitrile; at 20 ℃; for 3h;

With dihydrogen peroxide; In dichloromethane; acetonitrile; at -20 - 20 ℃; for 2.25h;
DOI:10.1016/j.tet.2006.04.071

Reference yield:

: 36314-51-9
(R)-1,2-bis-tetradecyloxy propane-3-ol

: 680220-11-5
2-O-benzyl-1,3-bis[(1,2-di-O-myristyl-sn-glycero-3)-phosphoryl]glycerol di(2-cyanoethyl) ester

Guidance literature:: Multi-step reaction with 2 steps

1.1: ethyldiisopropylamine / CH₂Cl₂ / 2 h / 20 °C

2.1: 1H-tetrazole / CH₂Cl₂; acetonitrile / 3 h / 20 °C

2.2: 7.1 g / hydrogen peroxide / CH₂Cl₂; acetonitrile / 2.25 h / -20 - 20 °C

With 1H-tetrazole; N-ethyl-N,N-diisopropylamine; In dichloromethane; acetonitrile;
DOI:10.1016/j.tet.2006.04.071

Reference yield: 88.0%

: 680220-11-5
2-O-benzyl-1,3-bis[(1,2-di-O-myristyl-sn-glycero-3)-phosphoryl]glycerol di(2-cyanoethyl) ester

: 2-O-benzyl-1,3-bis[(1,2-di-O-myristyl-sn-glycero-3)-phosphoryl]glycerol diammonium salt

Guidance literature:: 2-O-benzyl-1,3-bis[(1,2-di-O-myristyl-sn-glycero-3)-phosphoryl]glycerol di(2-cyanoethyl) ester; With triethylamine; In acetonitrile; at 20 ℃; for 24h;

With ammonium hydroxide;
DOI:10.1016/j.tet.2006.04.071