α,α,5,15-bis-α,α,10,20-bis(pivalamidophenyl)porphine

Base Information

Chemical Name:α,α,5,15-bis-α,α,10,20-bis(pivalamidophenyl)porphine
CAS No.:104070-04-4
Molecular Formula:C₇₄H₆₆N₁₂O₄
Molecular Weight:1187.42
Hs Code.:

α,α,5,15-bis<N-(-methylbenzimidazolyl)acetamidophenyl>-α,α,10,20-bis(pivalamidophenyl)porphine

Synonyms:α,α,5,15-bis-α,α,10,20-bis(pivalamidophenyl)porphine

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Chemical Property of α,α,5,15-bis-α,α,10,20-bis(pivalamidophenyl)porphine

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Technology Process of α,α,5,15-bis-α,α,10,20-bis(pivalamidophenyl)porphine

There total 6 articles about α,α,5,15-bis-α,α,10,20-bis(pivalamidophenyl)porphine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 104070-08-8
2-acetyl chloride

: 90703-83-6
N-(2-{(1Z,4Z,9Z,15Z)-10,20-Bis-(2-amino-phenyl)-15-[2-(2,2-dimethyl-propionylamino)-phenyl]-porphyrin-5-yl}-phenyl)-2,2-dimethyl-propionamide

: 104070-04-4
α,α,5,15-bis-α,α,10,20-bis(pivalamidophenyl)porphine

Guidance literature:: With pyridine; In N,N-dimethyl-formamide; Ambient temperature;
DOI:10.1021/ja00282a020

Reference yield:

: 52199-35-6
tetrakis-5,10,15,20-(o-aminophenyl)porphyrin

: 104070-04-4
α,α,5,15-bis-α,α,10,20-bis(pivalamidophenyl)porphine

Guidance literature:: Multi-step reaction with 2 steps

2: 96 percent / pyridine / dimethylformamide / Ambient temperature

With pyridine; In N,N-dimethyl-formamide;
DOI:10.1021/ja00282a020

Reference yield:

: 615-15-6
2-Methyl-1H-benzimidazole

: 104070-04-4
α,α,5,15-bis-α,α,10,20-bis(pivalamidophenyl)porphine

Guidance literature:: Multi-step reaction with 4 steps

1: 92 percent / 1.) sodium hydride / tetrahydrofuran / 1.) 3 h; 2.) 1 h, reflux

2: 76 percent / 48 percent HBr / H₂O / 0.5 h / Heating

3: thionyl chloride / dimethylformamide / 1 h / Ambient temperature

4: 96 percent / pyridine / dimethylformamide / Ambient temperature

With pyridine; thionyl chloride; hydrogen bromide; sodium hydride; In tetrahydrofuran; water; N,N-dimethyl-formamide;
DOI:10.1021/ja00282a020