N-(diphenylmethylene)-N-(1-naphthyl)amine

Base Information

• Chemical Name: N-(diphenylmethylene)-N-(1-naphthyl)amine
• CAS No.: 32566-86-2
• Molecular Formula: C₂₃H₁₇N
• Molecular Weight: 307.395
• Mol file: 32566-86-2.mol

Synonyms:benzhydrylidene-[1]naphthyl-amine

Chemical Property of N-(diphenylmethylene)-N-(1-naphthyl)amine

Chemical Property:

Purity/Quality:

N-(diphenylmethylene)-1-naphthalenamine ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N-(diphenylmethylene)-N-(1-naphthyl)amine

There total 11 articles about N-(diphenylmethylene)-N-(1-naphthyl)amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

Benzophenone imine (1013-88-3) + 1-Chloronaphthalene (90-13-1) → benzhydrylidene-[1]naphthyl-amine (32566-86-2)

Guidance literature:

With 1,8-bis(diisopropylphosphino)triptycene; potassium phosphate; palladium diacetate; In toluene;

DOI:10.1055/s-2008-1032142

Reference yield: 85.0%

Benzophenone imine (1013-88-3) + 1-naphthyl triflate (99747-74-7) → benzhydrylidene-[1]naphthyl-amine (32566-86-2)

Guidance literature:

With palladium diacetate; caesium carbonate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; In tetrahydrofuran; at 65 ℃; for 16h; Product distribution; var. aryl bromides and triflates; var. solv. temp and time; var reagents: Pd₂(dba)3, t-BuONa;

DOI:10.1016/S0040-4039(97)01465-2

Reference yield: 73.0%

benzophenone (119-61-9) + 1-amino-naphthalene (134-32-7) → benzhydrylidene-[1]naphthyl-amine (32566-86-2)

Guidance literature:

benzophenone; With titanium tetrachloride; In toluene; Reflux;

1-amino-naphthalene; In toluene; for 24h; Reflux;

DOI:10.1021/om501060f

upstream raw materials:

Benzophenone imine

1-amino-naphthalene

benzophenone

Dichlorodiphenylmethane

Downstream raw materials:

N-benzhydrylnaphthalen-1-amine

1-amino-naphthalene

N-α-Naphthyl-α-chloro-α,α-diphenylacetimidoylchlorid

Dimethyl meso-3,3-Diphenylcyclopropane-1,2-dicarboxylate