(±)-7-[²H₁]-benzyl phenyl thioether

Base Information

Chemical Name:(±)-7-[²H₁]-benzyl phenyl thioether
CAS No.:7693-39-2
Molecular Formula:C₁₃H₁₂S
Molecular Weight:201.296
Hs Code.:

(±)-7-[<sup>2</sup>H<sub>1</sub>]-benzyl phenyl thioether

Synonyms:(±)-7-[²H₁]-benzyl phenyl thioether

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Chemical Property of (±)-7-[²H₁]-benzyl phenyl thioether

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Technology Process of (±)-7-[²H₁]-benzyl phenyl thioether

There total 7 articles about (±)-7-[²H₁]-benzyl phenyl thioether which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 66343-88-2
racemic benzyl-α-d₁ bromide

: 108-98-5
thiophenol

: 7693-39-2
(±)-7-[²H₁]-benzyl phenyl thioether

Guidance literature:: With 1,8-diazabicyclo[5.4.0]undec-7-ene; In acetonitrile; at 20 ℃; for 18h; Inert atmosphere;
DOI:10.3762/bjoc.14.6

Reference yield:

: 831-91-4
Benzyl phenyl sulfide

: 7693-39-2
(±)-7-[²H₁]-benzyl phenyl thioether

Guidance literature:: Multi-step reaction with 2 steps

1: n-butyllithium / tetrahydrofuran; hexane / 1 h / -65 °C

2: D₂O

With n-butyllithium; water-d2; In tetrahydrofuran; hexane;
DOI:10.1016/0022-328X(88)80498-4

Reference yield:

: 100-39-0
benzyl bromide

: 7693-39-2
(±)-7-[²H₁]-benzyl phenyl thioether

Guidance literature:: Multi-step reaction with 3 steps

1: 97.5 percent / 5percent aqueous NaOH / 6 h / 100 °C

2: n-butyllithium / tetrahydrofuran; hexane / 1 h / -65 °C

3: D₂O

With sodium hydroxide; n-butyllithium; water-d2; In tetrahydrofuran; hexane;
DOI:10.1016/0022-328X(88)80498-4