8-Methoxyphenanthridin-6(5H)-one

Base Information

Chemical Name:8-Methoxyphenanthridin-6(5H)-one
CAS No.:38088-95-8
Molecular Formula:C₁₄H₁₁NO₂
Molecular Weight:225.247
Hs Code.:
DSSTox Substance ID:DTXSID60701400
Nikkaji Number:J113.800F
Wikidata:Q82633031
Mol file:38088-95-8.mol

Synonyms:8-Methoxyphenanthridin-6(5H)-one;38088-95-8;DTXSID60701400;8-Methoxy-6(5H)-phenanthridinone;6(5H)-Phenanthridinone, 8-methoxy-

Suppliers and Price of 8-Methoxyphenanthridin-6(5H)-one

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 3 raw suppliers

Chemical Property of 8-Methoxyphenanthridin-6(5H)-one

Chemical Property:

XLogP3:2.4
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:1
Exact Mass:225.078978594
Heavy Atom Count:17
Complexity:305

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:COC1=CC2=C(C=C1)C3=CC=CC=C3NC2=O

Technology Process of 8-Methoxyphenanthridin-6(5H)-one

There total 28 articles about 8-Methoxyphenanthridin-6(5H)-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: N-(tert-butyl)-4-methoxy-2′-pivalamido-[1,1′-biphenyl]-2-carboxamide

: 38088-95-8
8-methoxyphenanthridine-6(5H)-one

Guidance literature:: With toluene-4-sulfonic acid; In tert-butyl alcohol; at 140 ℃; for 24h; Schlenk technique; Inert atmosphere;
DOI:10.1021/acs.joc.0c02722

Reference yield: 94.0%

: 2446-83-5
di-isopropyl azodicarboxylate

: 1609211-13-3
N-(4′-methoxy-[1,1′-biphenyl]-2-yl)picolinamide

: 38088-95-8
8-methoxyphenanthridine-6(5H)-one

Guidance literature:: With oxygen; sodium pivalate; cobalt(II) chloride; In 1,4-dioxane; at 130 ℃; for 24h; under 760.051 Torr; regioselective reaction;
DOI:10.1021/acs.joc.8b00730

Reference yield: 92.0%

: 35450-36-3
methyl 2-bromo-5-methoxybenzoate

: 5570-18-3
2-aminophenylboronic acid

: 38088-95-8
8-methoxyphenanthridine-6(5H)-one

Guidance literature:: With dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; potassium phosphate; palladium diacetate; In 1,4-dioxane; water; at 100 ℃; for 24h; Inert atmosphere;
DOI:10.1016/j.tetlet.2013.05.022