2,2-Bis-dicyclohexylamino-1-methyl-4-phenyl-3-trimethylsilanyl-1H-2λ⁵-[1,5,2]diazaphosphinine-6-thione

Base Information

• Chemical Name: 2,2-Bis-dicyclohexylamino-1-methyl-4-phenyl-3-trimethylsilanyl-1H-2λ⁵-[1,5,2]diazaphosphinine-6-thione
• CAS No.: 200071-11-0
• Molecular Formula: C₃₇H₆₁N₄PSSi
• Molecular Weight: 653.043

Synonyms:2,2-Bis-dicyclohexylamino-1-methyl-4-phenyl-3-trimethylsilanyl-1H-2λ⁵-[1,5,2]diazaphosphinine-6-thione

Chemical Property of 2,2-Bis-dicyclohexylamino-1-methyl-4-phenyl-3-trimethylsilanyl-1H-2λ⁵-[1,5,2]diazaphosphinine-6-thione

Chemical Property:

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Technology Process of 2,2-Bis-dicyclohexylamino-1-methyl-4-phenyl-3-trimethylsilanyl-1H-2λ⁵-[1,5,2]diazaphosphinine-6-thione

There total 4 articles about 2,2-Bis-dicyclohexylamino-1-methyl-4-phenyl-3-trimethylsilanyl-1H-2λ⁵-[1,5,2]diazaphosphinine-6-thione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.0%

methyl thioisocyanate (556-61-6) + [2-Bis(dicyclohexylamino)-4-phenyl-2-trimethylsilyl]-2λ5-azaphosphete (167955-66-0) → 2,2-Bis-dicyclohexylamino-1-methyl-4-phenyl-3-trimethylsilanyl-1H-2λ5-[1,5,2]diazaphosphinine-6-thione (200071-11-0)

Guidance literature:

In toluene; at 50 ℃; for 60h;

DOI:10.1002/chem.19970031106

Reference yield:

[bis(dicyclohexylamino)phosphino](trimethylsilyl)carbene (152387-46-7,156280-08-9) → 2,2-Bis-dicyclohexylamino-1-methyl-4-phenyl-3-trimethylsilanyl-1H-2λ5-[1,5,2]diazaphosphinine-6-thione (200071-11-0)

Guidance literature:

Multi-step reaction with 3 steps

1: 85 percent / toluene / 18 h / Ambient temperature

2: 98 percent / pentane / 19 h / Irradiation

3: 56 percent / toluene / 60 h / 50 °C

In toluene; pentane;

DOI:10.1002/chem.19970031106

Reference yield:

3-phenyl-2,2-(bis(dicyclohexylamino)phosphino)(trimethylsilyl)-2H-aziridine (167955-65-9) → 2,2-Bis-dicyclohexylamino-1-methyl-4-phenyl-3-trimethylsilanyl-1H-2λ5-[1,5,2]diazaphosphinine-6-thione (200071-11-0)

Guidance literature:

Multi-step reaction with 2 steps

1: 98 percent / pentane / 19 h / Irradiation

2: 56 percent / toluene / 60 h / 50 °C

In toluene; pentane;

DOI:10.1002/chem.19970031106

upstream raw materials:

methyl thioisocyanate

[2-Bis(dicyclohexylamino)-4-phenyl-2-trimethylsilyl]-2λ⁵-azaphosphete

[Bis(dicyclohexylamino)phosphanyl](trimethylsilyl)diazomethane

[bis(dicyclohexylamino)phosphino](trimethylsilyl)carbene

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