1-<3,5-bis-O-(p-chlorobenzoyl)-2-deoxy-α-D-erythro-pentofuranosyl>-5-trifluoromethyluracil

Base Information

Chemical Name:1-<3,5-bis-O-(p-chlorobenzoyl)-2-deoxy-α-D-erythro-pentofuranosyl>-5-trifluoromethyluracil
CAS No.:129664-48-8
Molecular Formula:C₂₄H₁₇Cl₂F₃N₂O₇
Molecular Weight:573.309
Hs Code.:

Synonyms:1-<3,5-bis-O-(p-chlorobenzoyl)-2-deoxy-α-D-erythro-pentofuranosyl>-5-trifluoromethyluracil

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-<3,5-bis-O-(p-chlorobenzoyl)-2-deoxy-α-D-erythro-pentofuranosyl>-5-trifluoromethyluracil

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Technology Process of 1-<3,5-bis-O-(p-chlorobenzoyl)-2-deoxy-α-D-erythro-pentofuranosyl>-5-trifluoromethyluracil

There total 2 articles about 1-<3,5-bis-O-(p-chlorobenzoyl)-2-deoxy-α-D-erythro-pentofuranosyl>-5-trifluoromethyluracil which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 3601-90-9
5-chloro-2-(((4-chlorobenzoyl)oxy)methyl)tetrahydrofuran-3-yl 4-chlorobenzoate

: 7057-43-4
5-trifluoromethyl-2,4-bis(trimethylsilyloxy)pyrimidine

: 129664-47-7
1-<3,5-bis-O-(p-chlorobenzoyl)-2-deoxy-β-D-erythro-pentofuranosyl>-5-trifluoromethyluracil

: 129664-48-8
1-<3,5-bis-O-(p-chlorobenzoyl)-2-deoxy-α-D-erythro-pentofuranosyl>-5-trifluoromethyluracil

Guidance literature:: In chloroform; at 20 ℃; for 4h; Overall yield = 18.51 %; Overall yield = 2.48 g;

Reference yield:

: 21740-23-8
3,5-O-bis(4-chlorobenzoyl)-2-deoxy-α-D-ribofuranosyl chloride

: 7057-43-4
5-trifluoromethyl-2,4-bis(trimethylsilyloxy)pyrimidine

: 129664-47-7
1-<3,5-bis-O-(p-chlorobenzoyl)-2-deoxy-β-D-erythro-pentofuranosyl>-5-trifluoromethyluracil

: 129664-48-8
1-<3,5-bis-O-(p-chlorobenzoyl)-2-deoxy-α-D-erythro-pentofuranosyl>-5-trifluoromethyluracil

Guidance literature:: In chloroform; Product distribution; Ambient temperature; various equivalent of silylated 5-trifluorouracil to the sugar; addition of different catalysts;
DOI:10.3987/COM-90-5315