methyl (Z)-2-(3-hydroxy-4-(4-methoxyphenyl)-5-oxofuran-2(5H)-ylidene)-2-iodoacetate

Base Information

Chemical Name:methyl (Z)-2-(3-hydroxy-4-(4-methoxyphenyl)-5-oxofuran-2(5H)-ylidene)-2-iodoacetate
CAS No.:1158649-25-2
Molecular Formula:C₁₄H₁₁IO₆
Molecular Weight:402.142
Hs Code.:

Synonyms:methyl (Z)-2-(3-hydroxy-4-(4-methoxyphenyl)-5-oxofuran-2(5H)-ylidene)-2-iodoacetate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl (Z)-2-(3-hydroxy-4-(4-methoxyphenyl)-5-oxofuran-2(5H)-ylidene)-2-iodoacetate

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Technology Process of methyl (Z)-2-(3-hydroxy-4-(4-methoxyphenyl)-5-oxofuran-2(5H)-ylidene)-2-iodoacetate

There total 1 articles about methyl (Z)-2-(3-hydroxy-4-(4-methoxyphenyl)-5-oxofuran-2(5H)-ylidene)-2-iodoacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

: 1158649-28-5
methyl (Z)-2-(3-hydroxy-4-(4-methoxyphenyl)-5-oxofuran-2(5H)-ylidene)acetate

: 1158649-25-2
methyl (Z)-2-(3-hydroxy-4-(4-methoxyphenyl)-5-oxofuran-2(5H)-ylidene)-2-iodoacetate

Guidance literature:: methyl (Z)-2-(3-hydroxy-4-(4-methoxyphenyl)-5-oxofuran-2(5H)-ylidene)acetate; With water; sodium hydroxide; In acetone; at 20 ℃; for 2h; Inert atmosphere;

With N-iodo-succinimide; acetic acid; In tetrahydrofuran; at 50 ℃; for 16h; Inert atmosphere;
DOI:10.1016/j.bmc.2010.09.037

Reference yield: 81.0%

: 1158649-25-2
methyl (Z)-2-(3-hydroxy-4-(4-methoxyphenyl)-5-oxofuran-2(5H)-ylidene)-2-iodoacetate

: 24388-23-6
2-phenyl-4,4,5,5-tetramethyl-1,3,2-dioxoborole

: 481-64-1
(E)-4-hydroxy-5-(α-methoxycarbonylbenzylidene)-3-(4-methoxyphenyl)furan-2(5H)-one

Guidance literature:: With bis(triphenylphosphine)palladium(II)-chloride; sodium carbonate; In tetrahydrofuran; water; for 2h; Inert atmosphere; Reflux;
DOI:10.1016/j.tetlet.2009.03.011

Reference yield: 80.0%

: 1073339-21-5
4,4,5,5-tetramethyl-2-(2-(trifluoromethyl)phenyl)-1,3,2-dioxaborolane

: 1158649-25-2
methyl (Z)-2-(3-hydroxy-4-(4-methoxyphenyl)-5-oxofuran-2(5H)-ylidene)-2-iodoacetate

: 1158649-32-1
methyl (E)-2-(3-hydroxy-4-(4-methoxyphenyl)-5-oxofuran-2(5H)-ylidene)-2-(2-(trifluoromethyl)phenyl)acetate

Guidance literature:: With bis(triphenylphosphine)palladium(II)-chloride; sodium carbonate; In tetrahydrofuran; water; for 2h; Inert atmosphere; Reflux;
DOI:10.1016/j.tetlet.2009.03.011