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[(HC(C(CH3)N(2,6-iPrC6H3))2)Ga(OH)(Me)]

Base Information
  • Chemical Name:[(HC(C(CH3)N(2,6-iPrC6H3))2)Ga(OH)(Me)]
  • CAS No.:877123-13-2
  • Molecular Formula:C30H45GaN2O
  • Molecular Weight:519.423
  • Hs Code.:
[(HC(C(CH<sub>3</sub>)N(2,6-iPrC<sub>6</sub>H<sub>3</sub>))2)Ga(OH)(Me)]

Synonyms:[(HC(C(CH3)N(2,6-iPrC6H3))2)Ga(OH)(Me)]

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Chemical Property of [(HC(C(CH3)N(2,6-iPrC6H3))2)Ga(OH)(Me)]
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Technology Process of [(HC(C(CH3)N(2,6-iPrC6H3))2)Ga(OH)(Me)]

There total 1 articles about [(HC(C(CH3)N(2,6-iPrC6H3))2)Ga(OH)(Me)] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
With 1,3-di-tert-butylimidazol-2-ylidene; In toluene; byproducts: 1,3-di-tert-butylimidazolium chloride; to soln. Ga complex and 1,3-di-tert-butylimidazol-2-ylidene in toluene 1equiv. water was added over 30 min and stirred for 15 min; volatiles were removed in vacuo, residue was extd. with n-hexane, concd., and stored at -20°C for 2 days; elem. anal.;
DOI:10.1021/ic051769l
Guidance literature:
In toluene; byproducts: methane; toluene was added at 0°C to kixt. Ga and Zr complexes and stirredfor 2 h at room temp. and for 24 h at 100°C; soln. was kept at room temp. for 48 h; elem. anal.;
DOI:10.1021/ic051769l
Guidance literature:
In toluene; toluene added to an mixt. (excess of Li compd.) at -78°C, stirredat room temp. for 12 h; elem. anal.;
DOI:10.1039/b712240c
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