Technology Process of C23H35N7O7S
There total 15 articles about C23H35N7O7S which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 6 steps
1: 99 percent / NaHCO3 / tetrahydrofuran / 0 - 20 °C
2: 1.) LiHMDS / 1.) THF, RT, 2.) THF, from 0 deg C to RT
3: 100 percent / HCl / ethyl acetate / 0 - 20 °C
4: Et3N / acetonitrile / 0 - 20 °C
5: 95 percent / aq. LiOH / ethanol / 0 - 20 °C
6: EDC, HOBt, DIPEA / acetonitrile
With
hydrogenchloride; lithium hydroxide; sodium hydrogencarbonate; benzotriazol-1-ol; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; triethylamine; N-ethyl-N,N-diisopropylamine; lithium hexamethyldisilazane;
In
tetrahydrofuran; ethanol; ethyl acetate; acetonitrile;
DOI:10.1021/jm960572n
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 1.) LiHMDS / 1.) THF, RT, 2.) THF, from 0 deg C to RT
2: 100 percent / HCl / ethyl acetate / 0 - 20 °C
3: Et3N / acetonitrile / 0 - 20 °C
4: 95 percent / aq. LiOH / ethanol / 0 - 20 °C
5: EDC, HOBt, DIPEA / acetonitrile
With
hydrogenchloride; lithium hydroxide; benzotriazol-1-ol; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; triethylamine; N-ethyl-N,N-diisopropylamine; lithium hexamethyldisilazane;
In
ethanol; ethyl acetate; acetonitrile;
DOI:10.1021/jm960572n
- Guidance literature:
-
Multi-step reaction with 3 steps
1: Et3N / acetonitrile / 0 - 20 °C
2: 95 percent / aq. LiOH / ethanol / 0 - 20 °C
3: EDC, HOBt, DIPEA / acetonitrile
With
lithium hydroxide; benzotriazol-1-ol; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; triethylamine; N-ethyl-N,N-diisopropylamine;
In
ethanol; acetonitrile;
DOI:10.1021/jm960572n