(2R,3S)-2,3-bis<4-(tert-butyldimethylsiloxy)phenyl>pentyl 3-hydroxypropyl sulfide

Base Information

Chemical Name:(2R*,3S*)-2,3-bis<4-(tert-butyldimethylsiloxy)phenyl>pentyl 3-hydroxypropyl sulfide
CAS No.:107036-30-6
Molecular Formula:C₃₂H₅₄O₃SSi₂
Molecular Weight:575.016
Hs Code.:

Synonyms:(2R*,3S*)-2,3-bis<4-(tert-butyldimethylsiloxy)phenyl>pentyl 3-hydroxypropyl sulfide

Suppliers and Price of (2R*,3S*)-2,3-bis<4-(tert-butyldimethylsiloxy)phenyl>pentyl 3-hydroxypropyl sulfide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2R*,3S*)-2,3-bis<4-(tert-butyldimethylsiloxy)phenyl>pentyl 3-hydroxypropyl sulfide

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Technology Process of (2R*,3S*)-2,3-bis<4-(tert-butyldimethylsiloxy)phenyl>pentyl 3-hydroxypropyl sulfide

There total 2 articles about (2R*,3S*)-2,3-bis<4-(tert-butyldimethylsiloxy)phenyl>pentyl 3-hydroxypropyl sulfide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.6%

: 107036-29-3
(2R*,3S*)-2,3-bis<4-(tert-butyldimethylsiloxy)phenyl>pentyl 2-carbomethoxyethyl sulfide

: 107036-30-6
(2R*,3S*)-2,3-bis<4-(tert-butyldimethylsiloxy)phenyl>pentyl 3-hydroxypropyl sulfide

Guidance literature:: With lithium aluminium tetrahydride; In tetrahydrofuran; for 0.333333h;
DOI:10.1021/jm00388a015

Reference yield:

: 104946-98-7
(2R*,3S*)-2,3-bis<4-<(tert-butyldimethylsilyl)oxy>phenyl>-1-pentanethiol

: 107036-30-6
(2R*,3S*)-2,3-bis<4-(tert-butyldimethylsiloxy)phenyl>pentyl 3-hydroxypropyl sulfide

Guidance literature:: Multi-step reaction with 2 steps

1: 79.4 percent / sodium methoxide / dioxane / 1 h / 45 °C

2: 60.6 percent / LiAlH₄ / tetrahydrofuran / 0.33 h

With lithium aluminium tetrahydride; sodium methylate; In tetrahydrofuran; 1,4-dioxane;
DOI:10.1021/jm00388a015