tert-butyl 11-(4-(benzyloxy)phenyloxy)undecanoate

Base Information

Chemical Name:tert-butyl 11-(4-(benzyloxy)phenyloxy)undecanoate
CAS No.:405157-50-8
Molecular Formula:C₂₈H₄₀O₄
Molecular Weight:440.623
Hs Code.:

Synonyms:tert-butyl 11-(4-(benzyloxy)phenyloxy)undecanoate

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Chemical Property of tert-butyl 11-(4-(benzyloxy)phenyloxy)undecanoate

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Technology Process of tert-butyl 11-(4-(benzyloxy)phenyloxy)undecanoate

There total 1 articles about tert-butyl 11-(4-(benzyloxy)phenyloxy)undecanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2834-05-1
11-bromoundecanoic acid

: 405157-50-8
tert-butyl 11-(4-(benzyloxy)phenyloxy)undecanoate

Guidance literature:: Multi-step reaction with 2 steps

1: 90 percent / conc. H₂SO₄ / CH₂Cl₂ / 15 h / 20 °C

2: 92 percent / K₂CO₃ / 18-crown-6 / acetone / 36 h / 60 °C

With sulfuric acid; potassium carbonate; 18-crown-6 ether; In dichloromethane; acetone;
DOI:10.1021/ma010290j

Reference yield: 98.0%

: 405157-50-8
tert-butyl 11-(4-(benzyloxy)phenyloxy)undecanoate

: 405157-52-0
tert-butyl 11-(4-hydroxy-phenyloxy)undecanoate

Guidance literature:: With hydrogen; palladium on activated charcoal; In ethyl acetate; at 20 ℃;
DOI:10.1021/ma010290j

Reference yield:

: 405157-50-8
tert-butyl 11-(4-(benzyloxy)phenyloxy)undecanoate

: 405157-55-3
4''-[10-(hydroxycarbonyl)decyloxy]phenyl 4-[4'-(2-(R)-octyloxy)-3'-nitrophenyl]benzoate

Guidance literature:: Multi-step reaction with 3 steps

1: 98 percent / H₂ / 10 percent Pd/C / ethyl acetate / 20 °C

2: 72 percent / N,N'-dicyclohexylcarbodiimide; 4-(dimethylamino)pyridine / CH₂Cl₂ / 24 h / 20 °C

3: 95 percent / trifluoroacetic acid / CH₂Cl₂ / 13 h

With dmap; hydrogen; dicyclohexyl-carbodiimide; trifluoroacetic acid; palladium on activated charcoal; In dichloromethane; ethyl acetate;
DOI:10.1021/ma010290j