Technology Process of tert-butyl 11-(4-hydroxy-phenyloxy)undecanoate
There total 4 articles about tert-butyl 11-(4-hydroxy-phenyloxy)undecanoate which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
hydrogen;
palladium on activated charcoal;
In
ethyl acetate;
at 20 ℃;
DOI:10.1021/ma010290j
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 92 percent / K2CO3 / 18-crown-6 / acetone / 36 h / 60 °C
2: 98 percent / H2 / 10 percent Pd/C / ethyl acetate / 20 °C
With
hydrogen; potassium carbonate;
palladium on activated charcoal; 18-crown-6 ether;
In
ethyl acetate; acetone;
DOI:10.1021/ma010290j
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 90 percent / conc. H2SO4 / CH2Cl2 / 15 h / 20 °C
2: 92 percent / K2CO3 / 18-crown-6 / acetone / 36 h / 60 °C
3: 98 percent / H2 / 10 percent Pd/C / ethyl acetate / 20 °C
With
sulfuric acid; hydrogen; potassium carbonate;
palladium on activated charcoal; 18-crown-6 ether;
In
dichloromethane; ethyl acetate; acetone;
DOI:10.1021/ma010290j
