methyl 4-(5-(benzo[d][1,3]dioxol-5-yl)-1,3,4-oxadiazol-2-ylthio)methyl benzoate

Base Information

Chemical Name:methyl 4-(5-(benzo[d][1,3]dioxol-5-yl)-1,3,4-oxadiazol-2-ylthio)methyl benzoate
CAS No.:875456-04-5
Molecular Formula:C₁₈H₁₄N₂O₅S
Molecular Weight:370.386
Hs Code.:

Synonyms:methyl 4-(5-(benzo[d][1,3]dioxol-5-yl)-1,3,4-oxadiazol-2-ylthio)methyl benzoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl 4-(5-(benzo[d][1,3]dioxol-5-yl)-1,3,4-oxadiazol-2-ylthio)methyl benzoate

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Technology Process of methyl 4-(5-(benzo[d][1,3]dioxol-5-yl)-1,3,4-oxadiazol-2-ylthio)methyl benzoate

There total 4 articles about methyl 4-(5-(benzo[d][1,3]dioxol-5-yl)-1,3,4-oxadiazol-2-ylthio)methyl benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 2417-72-3
Methyl 4-(bromomethyl)benzoate

: 63698-52-2
2-mercapto-5-(3,4-methylenedioxyphenyl)-1,3,4-oxadiazole

: 875456-04-5
methyl 4-(5-(benzo[d][1,3]dioxol-5-yl)-1,3,4-oxadiazol-2-ylthio)methyl benzoate

Guidance literature:: With sodium hydroxide; In N,N-dimethyl-formamide; at 20 ℃; for 5h; Inert atmosphere;
DOI:10.1021/jm300309a

Reference yield:

: 94-53-1
Piperonylic acid

: 875456-04-5
methyl 4-(5-(benzo[d][1,3]dioxol-5-yl)-1,3,4-oxadiazol-2-ylthio)methyl benzoate

Guidance literature:: Multi-step reaction with 4 steps

1: 13 h / 0 - 50 °C

2: hydrazine hydrate / ethanol / 48 h / Reflux

3: triethylamine / ethanol / Reflux; Inert atmosphere

4: sodium hydroxide / N,N-dimethyl-formamide / 5 h / 20 °C / Inert atmosphere

With hydrazine hydrate; triethylamine; sodium hydroxide; In ethanol; N,N-dimethyl-formamide;
DOI:10.1021/jm300309a

Reference yield:

: 22026-39-7
benzo[d][1,3]dioxole-5-carbohydrazide

: 875456-04-5
methyl 4-(5-(benzo[d][1,3]dioxol-5-yl)-1,3,4-oxadiazol-2-ylthio)methyl benzoate

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / ethanol / Reflux; Inert atmosphere

2: sodium hydroxide / N,N-dimethyl-formamide / 5 h / 20 °C / Inert atmosphere

With triethylamine; sodium hydroxide; In ethanol; N,N-dimethyl-formamide;
DOI:10.1021/jm300309a