methyl 4,6-O-benzylidene-2,3-dideoxy-2-nitro-β-D-erythro hex-2-enopyranoside

Base Information

Chemical Name:methyl 4,6-O-benzylidene-2,3-dideoxy-2-nitro-β-D-erythro hex-2-enopyranoside
CAS No.:85761-14-4
Molecular Formula:C₁₄H₁₅NO₆
Molecular Weight:293.276
Hs Code.:

Synonyms:methyl 4,6-O-benzylidene-2,3-dideoxy-2-nitro-β-D-erythro hex-2-enopyranoside

Suppliers and Price of methyl 4,6-O-benzylidene-2,3-dideoxy-2-nitro-β-D-erythro hex-2-enopyranoside

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of methyl 4,6-O-benzylidene-2,3-dideoxy-2-nitro-β-D-erythro hex-2-enopyranoside

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of methyl 4,6-O-benzylidene-2,3-dideoxy-2-nitro-β-D-erythro hex-2-enopyranoside

There total 2 articles about methyl 4,6-O-benzylidene-2,3-dideoxy-2-nitro-β-D-erythro hex-2-enopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 92841-79-7
methyl 4,6-O-benzylidene-2-deoxy-2-nitro-β-D-glucopyranoside

: 85761-14-4
methyl 4,6-O-benzylidene-2,3-dideoxy-2-nitro-β-D-erythro hex-2-enopyranoside

Guidance literature:: With methanesulfonyl chloride; triethylamine; In tetrahydrofuran; for 0.75h; Ambient temperature;
DOI:10.1016/S0040-4020(01)91801-0

Reference yield:

: 61664-96-8
methyl 4,6-O-benzylidene-2,3-dideoxy-3-C-nitro-β-D-hex-2-enepyranoside

: 85761-14-4
methyl 4,6-O-benzylidene-2,3-dideoxy-2-nitro-β-D-erythro hex-2-enopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 57 percent / sodium nitrite / tributylhexadecylphosphonium bromide / benzene; H₂O / 2 h / Ambient temperature

2: 85 percent / methanesulphonyl chloride, Et₃N / tetrahydrofuran / 0.75 h / Ambient temperature

With methanesulfonyl chloride; triethylamine; sodium nitrite; cetyltributylphosphonium bromide; In tetrahydrofuran; water; benzene;
DOI:10.1016/S0040-4020(01)91801-0