C₂₃H₂₇NO₆S

Base Information

Chemical Name:C₂₃H₂₇NO₆S
CAS No.:1360464-24-9
Molecular Formula:C₂₃H₂₇NO₆S
Molecular Weight:445.536
Hs Code.:

C<sub>23</sub>H<sub>27</sub>NO<sub>6</sub>S

Synonyms:C₂₃H₂₇NO₆S

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₃H₂₇NO₆S

Chemical Property:

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Technology Process of C₂₃H₂₇NO₆S

There total 8 articles about C₂₃H₂₇NO₆S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 1360464-23-8
C₂₃H₂₇NO₄S

: 1360464-24-9
C₂₃H₂₇NO₆S

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; In dichloromethane;
DOI:10.1016/j.bmcl.2011.12.057

Reference yield:

: 4746-97-8
cyclohexanedione monoethylene ketal

: 1360464-24-9
C₂₃H₂₇NO₆S

Guidance literature:: Multi-step reaction with 9 steps

1: sodium hydride / tetrahydrofuran / Reflux

2: ytterbium(III) triflate / benzene / Reflux

3: sodium tris(acetoxy)borohydride; acetic acid / acetonitrile

4: sodium t-butanolate / tetrahydrofuran

5: lithium aluminium tetrahydride / diethyl ether

6: 20% palladium hydroxide on charcoal; hydrogen / methanol

7: potassium carbonate / dichloromethane

8: tributylphosphine / acetonitrile

9: 3-chloro-benzenecarboperoxoic acid / dichloromethane

With lithium aluminium tetrahydride; tributylphosphine; 20% palladium hydroxide on charcoal; hydrogen; sodium tris(acetoxy)borohydride; sodium hydride; potassium carbonate; acetic acid; 3-chloro-benzenecarboperoxoic acid; sodium t-butanolate; ytterbium(III) triflate; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; acetonitrile; benzene;
DOI:10.1016/j.bmcl.2011.12.057

Reference yield:

: 813445-20-4
(7R,8R)-8-((R)-1-phenyl-ethylamino)-1,4-dioxa-spiro[4.5]decane-7-carboxylic acid ethyl ester

: 1360464-24-9
C₂₃H₂₇NO₆S

Guidance literature:: Multi-step reaction with 5 steps

1: lithium aluminium tetrahydride / diethyl ether

2: 20% palladium hydroxide on charcoal; hydrogen / methanol

3: potassium carbonate / dichloromethane

4: tributylphosphine / acetonitrile

5: 3-chloro-benzenecarboperoxoic acid / dichloromethane

With lithium aluminium tetrahydride; tributylphosphine; 20% palladium hydroxide on charcoal; hydrogen; potassium carbonate; 3-chloro-benzenecarboperoxoic acid; In methanol; diethyl ether; dichloromethane; acetonitrile;
DOI:10.1016/j.bmcl.2011.12.057