(R)-ethyl 3-methyl-5-phenyl-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)pentanethioate

Base Information

Chemical Name:(R)-ethyl 3-methyl-5-phenyl-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)pentanethioate
CAS No.:1239568-91-2
Molecular Formula:C₂₀H₃₁BO₃S
Molecular Weight:362.341
Hs Code.:

Synonyms:(R)-ethyl 3-methyl-5-phenyl-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)pentanethioate

Suppliers and Price of (R)-ethyl 3-methyl-5-phenyl-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)pentanethioate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of (R)-ethyl 3-methyl-5-phenyl-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)pentanethioate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (R)-ethyl 3-methyl-5-phenyl-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)pentanethioate

There total 1 articles about (R)-ethyl 3-methyl-5-phenyl-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)pentanethioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 1239568-98-9
(E)-ethyl 3-methyl-5-phenylpent-2-enethioate

: 73183-34-3
bis(pinacol)diborane

: 1239568-91-2
(R)-ethyl 3-methyl-5-phenyl-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)pentanethioate

Guidance literature:: (E)-ethyl 3-methyl-5-phenylpent-2-enethioate; bis(pinacol)diborane; With methanol; (Ph₂C₃H₂N₂(C₆H₄Ph)(C₆H₂iPr₃))Cu(Ot-Bu); In tetrahydrofuran; at -50 ℃; for 18h; Inert atmosphere;

With hydrogenchloride; In tetrahydrofuran; methanol; water; at -50 - 22 ℃; optical yield given as %ee; enantioselective reaction; Inert atmosphere;
DOI:10.1021/ja104777u