5-Chloro-2,2,3,3,4,4,5,5-octafluoro-N-(4-methoxy-phenyl)-pentanimidoyl iodide

Base Information

Chemical Name:5-Chloro-2,2,3,3,4,4,5,5-octafluoro-N-(4-methoxy-phenyl)-pentanimidoyl iodide
CAS No.:183209-28-1
Molecular Formula:C₁₂H₇ClF₈INO
Molecular Weight:495.538
Hs Code.:

Synonyms:5-Chloro-2,2,3,3,4,4,5,5-octafluoro-N-(4-methoxy-phenyl)-pentanimidoyl iodide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 5-Chloro-2,2,3,3,4,4,5,5-octafluoro-N-(4-methoxy-phenyl)-pentanimidoyl iodide

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Technology Process of 5-Chloro-2,2,3,3,4,4,5,5-octafluoro-N-(4-methoxy-phenyl)-pentanimidoyl iodide

There total 1 articles about 5-Chloro-2,2,3,3,4,4,5,5-octafluoro-N-(4-methoxy-phenyl)-pentanimidoyl iodide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 5848-38-4
1-chloro-4-iodo-1,1,2,2,3,3,4,4-octafluorobutane

: 10349-38-9
p-methoxyphenylisonitrile

: 183209-28-1
5-Chloro-2,2,3,3,4,4,5,5-octafluoro-N-(4-methoxy-phenyl)-pentanimidoyl iodide

Guidance literature:: With sodium dithionite; sodium carbonate; In water; acetonitrile; at 10 - 15 ℃; for 0.666667h;
DOI:10.1016/0040-4039(96)01808-4

Reference yield: 89.0%

: 536-74-3
phenylacetylene

: 183209-28-1
5-Chloro-2,2,3,3,4,4,5,5-octafluoro-N-(4-methoxy-phenyl)-pentanimidoyl iodide

: 204130-89-2
[5-Chloro-2,2,3,3,4,4,5,5-octafluoro-1-phenylethynyl-pent-(E)-ylidene]-(4-methoxy-phenyl)-amine

Guidance literature:: With triethylamine; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; In acetonitrile; for 1h; Heating;
DOI:10.1016/S0022-1139(97)00119-X

Reference yield: 68.0%

: 98-86-2
acetophenone

: 183209-28-1
5-Chloro-2,2,3,3,4,4,5,5-octafluoro-N-(4-methoxy-phenyl)-pentanimidoyl iodide

: 197508-13-7
(E)-7-Chloro-4,4,5,5,6,6,7,7-octafluoro-3-(4-methoxy-phenylamino)-1-phenyl-hept-2-en-1-one

Guidance literature:: With sodium hydride; In tetrahydrofuran; for 0.333333h; Ambient temperature; 1.) 20 min, 2.) 15 min;
DOI:10.1016/S0022-1139(97)00027-4