benzyl-<1-(tert.-butyldimethylsilyloxymethyl)-allyl>-(2-propinyl)-amine

Base Information

Chemical Name:benzyl-<1-(tert.-butyldimethylsilyloxymethyl)-allyl>-(2-propinyl)-amine
CAS No.:160695-30-7
Molecular Formula:C₂₀H₃₁NOSi
Molecular Weight:329.558
Hs Code.:

Synonyms:benzyl-<1-(tert.-butyldimethylsilyloxymethyl)-allyl>-(2-propinyl)-amine

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Chemical Property of benzyl-<1-(tert.-butyldimethylsilyloxymethyl)-allyl>-(2-propinyl)-amine

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Technology Process of benzyl-<1-(tert.-butyldimethylsilyloxymethyl)-allyl>-(2-propinyl)-amine

There total 5 articles about benzyl-<1-(tert.-butyldimethylsilyloxymethyl)-allyl>-(2-propinyl)-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 50838-63-6,53214-59-8
2-Benzylamino-3-buten-1-ol

: 160695-30-7
benzyl-<1-(tert.-butyldimethylsilyloxymethyl)-allyl>-(2-propinyl)-amine

Guidance literature:: Multi-step reaction with 2 steps

1: 99 percent / imidazole / dimethylformamide / 0 deg C, 30 min then r.t., 3 h

2: 1.) NaH / 1.) THF, r.t., 30 min; 2.) THF, r.t. then reflux, 20 h

With 1H-imidazole; sodium hydride; In N,N-dimethyl-formamide;
DOI:10.1016/0040-4039(94)88505-2

Reference yield:

: 98-88-4
benzoyl chloride

: 160695-30-7
benzyl-<1-(tert.-butyldimethylsilyloxymethyl)-allyl>-(2-propinyl)-amine

Guidance literature:: Multi-step reaction with 4 steps

1: 50 percent / NaHCO₃ / H₂O; CH₂Cl₂ / 0.5 h / Ambient temperature

2: 93 percent / LiAlH₄ / diethyl ether / 14 h / Heating

3: 99 percent / imidazole / dimethylformamide / 0 deg C, 30 min then r.t., 3 h

4: 1.) NaH / 1.) THF, r.t., 30 min; 2.) THF, r.t. then reflux, 20 h

With 1H-imidazole; lithium aluminium tetrahydride; sodium hydride; sodium hydrogencarbonate; In diethyl ether; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1016/0040-4039(94)88505-2

Reference yield:

: 119768-88-6
N-benzoyl vinyl glycine methyl ester

: 160695-30-7
benzyl-<1-(tert.-butyldimethylsilyloxymethyl)-allyl>-(2-propinyl)-amine

Guidance literature:: Multi-step reaction with 3 steps

1: 93 percent / LiAlH₄ / diethyl ether / 14 h / Heating

2: 99 percent / imidazole / dimethylformamide / 0 deg C, 30 min then r.t., 3 h

3: 1.) NaH / 1.) THF, r.t., 30 min; 2.) THF, r.t. then reflux, 20 h

With 1H-imidazole; lithium aluminium tetrahydride; sodium hydride; In diethyl ether; N,N-dimethyl-formamide;
DOI:10.1016/0040-4039(94)88505-2