2-[(2',6'-dichlorophenyl)amino]phenyl acetoxyacetyl hydrazide

Base Information

Chemical Name:2-[(2',6'-dichlorophenyl)amino]phenyl acetoxyacetyl hydrazide
CAS No.:1332717-20-0
Molecular Formula:C₁₆H₁₅Cl₂N₃O₃
Molecular Weight:368.219
Hs Code.:

Synonyms:2-[(2',6'-dichlorophenyl)amino]phenyl acetoxyacetyl hydrazide

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Chemical Property of 2-[(2',6'-dichlorophenyl)amino]phenyl acetoxyacetyl hydrazide

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Technology Process of 2-[(2',6'-dichlorophenyl)amino]phenyl acetoxyacetyl hydrazide

There total 1 articles about 2-[(2',6'-dichlorophenyl)amino]phenyl acetoxyacetyl hydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 89796-99-6
aceclofenac

: 1332717-20-0
2-[(2',6'-dichlorophenyl)amino]phenyl acetoxyacetyl hydrazide

Guidance literature:: Multi-step reaction with 2 steps

1: sulfuric acid / Reflux

2: hydrazine hydrate / ethanol / Reflux

With hydrazine hydrate; sulfuric acid; In ethanol;
DOI:10.1007/s00044-010-9494-z

Reference yield: 81.0%

: 544693-22-3
2,3,4,4a-tetrahydro-1H-xanthen-1-one

: 1332717-20-0
2-[(2',6'-dichlorophenyl)amino]phenyl acetoxyacetyl hydrazide

: (E)-2-oxo-2-(2-(2,3,4,4a-tetrahydro-1H-xanthen-1-ylidene)hydrazinyl)ethyl-2-(2-((2,6-dichlorophenyl)amino)phenyl)acetate

Guidance literature:: With acetic acid; In ethanol; for 8h; Reflux;
DOI:10.1016/j.bioorg.2018.11.053

Reference yield:

: 1332717-20-0
2-[(2',6'-dichlorophenyl)amino]phenyl acetoxyacetyl hydrazide

: 1262801-24-0
[5-(2-oxo-2-(2-oxo-2H-chromen-3-yl)ethylthio)-1,3,4-oxadiazol-2-yl]methyl [2-{(2,6-dichlorophenyl)amino}phenyl]acetate

Guidance literature:: Multi-step reaction with 2 steps

1.1: potassium hydroxide / methanol / 12 h / Reflux

2.1: sodium ethanolate / ethanol / 4 h / Reflux

2.2: Reflux

With sodium ethanolate; potassium hydroxide; In methanol; ethanol;
DOI:10.1007/s00044-010-9494-z