(2R,4R)-4-(tert-Butyl-dimethyl-silanyloxy)-2,5-bis-(tert-butyl-diphenyl-silanyloxy)-pentanoic acid (2-allyl-phenyl)-amide

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Chemical Name:(2R,4R)-4-(tert-Butyl-dimethyl-silanyloxy)-2,5-bis-(tert-butyl-diphenyl-silanyloxy)-pentanoic acid (2-allyl-phenyl)-amide
CAS No.:114904-27-7
Molecular Formula:C₅₂H₆₉NO₄Si₃
Molecular Weight:856.381
Hs Code.:

Synonyms:(2R,4R)-4-(tert-Butyl-dimethyl-silanyloxy)-2,5-bis-(tert-butyl-diphenyl-silanyloxy)-pentanoic acid (2-allyl-phenyl)-amide

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Chemical Property of (2R,4R)-4-(tert-Butyl-dimethyl-silanyloxy)-2,5-bis-(tert-butyl-diphenyl-silanyloxy)-pentanoic acid (2-allyl-phenyl)-amide

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Technology Process of (2R,4R)-4-(tert-Butyl-dimethyl-silanyloxy)-2,5-bis-(tert-butyl-diphenyl-silanyloxy)-pentanoic acid (2-allyl-phenyl)-amide

There total 6 articles about (2R,4R)-4-(tert-Butyl-dimethyl-silanyloxy)-2,5-bis-(tert-butyl-diphenyl-silanyloxy)-pentanoic acid (2-allyl-phenyl)-amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 18162-48-6
tert-butyldimethylsilyl chloride

: 114877-80-4
(2S,4S)-2,5-Bis-(tert-butyl-diphenyl-silanyloxy)-4-hydroxy-pentanoic acid (2-allyl-phenyl)-amide

: 114904-27-7
(2S,4S)-4-(tert-Butyl-dimethyl-silanyloxy)-2,5-bis-(tert-butyl-diphenyl-silanyloxy)-pentanoic acid (2-allyl-phenyl)-amide

Guidance literature:: DOI:10.1021/jo00275a015

Reference yield: 75.0%

: 114877-80-4
(2R,4R)-2,5-Bis-(tert-butyl-diphenyl-silanyloxy)-4-hydroxy-pentanoic acid (2-allyl-phenyl)-amide

: 18162-48-6
tert-butyldimethylsilyl chloride

: 114904-27-7
(2R,4R)-4-(tert-Butyl-dimethyl-silanyloxy)-2,5-bis-(tert-butyl-diphenyl-silanyloxy)-pentanoic acid (2-allyl-phenyl)-amide

Guidance literature:: With 1H-imidazole; In N,N-dimethyl-formamide;
DOI:10.1016/S0040-4039(00)95503-5

Reference yield:

: 32704-22-6
2-allyl-phenylamine

: 114904-27-7
(2R,4R)-4-(tert-Butyl-dimethyl-silanyloxy)-2,5-bis-(tert-butyl-diphenyl-silanyloxy)-pentanoic acid (2-allyl-phenyl)-amide

Guidance literature:: Multi-step reaction with 2 steps

1: 81 percent / dimethylaluminum chloride / CH₂Cl₂ / Ambient temperature

2: 75 percent / imidazole / dimethylformamide

With 1H-imidazole; dimethylaluminum chloride; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/S0040-4039(00)95503-5